|
|||||
|
|
| 水热合成具有针尖状末端结构的哑铃状ZnO微晶 | |
| 引用本文： | 靳斌斌,刘延忠,闫晓前,王丹军.水热合成具有针尖状末端结构的哑铃状ZnO微晶[J].延安大学学报(自然科学版),2011,30(3):60-63. |
| 作者姓名： | 靳斌斌 刘延忠 闫晓前 王丹军 |
| 作者单位： | 1. 陕西国防工业职业技术学院化学工程系,陕西西安,710300 2. 延安油田股份有限公司西区采油厂,陕西延安,717500 3. 延安大学化学与化工学院,陕西延安,716000 |
| 基金项目： | 陕西国防工业职业技术学院研究与开发项目，陕西省教育厅科研基金项目 |
| 摘 要： | 以硝酸锌和氢氧化钠为原料,油酸钠作为形貌控制剂,在醇水体系中采用简单的水热法,于230℃制备出了针尖状哑铃氧化锌。采用X-射线粉末衍射(XRD)和扫描电子显微镜(SEM)对其结构和形貌进行了表征,并对其生长机理进行了探讨。 |
| 关 键 词： | 哑铃状 氧化锌微晶 水热合成 形貌控制剂 |
Hydrothermal Synthesis of Dumbbell-like Zinc Oxide Microcrystal with Sharp Tips |
|
| JIN Bin-bin,LIU Yan-zhong,YAN Xiao-qian,WANG Dan-jun.Hydrothermal Synthesis of Dumbbell-like Zinc Oxide Microcrystal with Sharp Tips[J].Journal of Yan'an University(Natural Science Edition),2011,30(3):60-63. | |
| Authors: | JIN Bin-bin LIU Yan-zhong YAN Xiao-qian WANG Dan-jun |
| Institution: | JIN Bin-bin1,LIU Yan-zhong2,YAN Xiao-qian1,WANG Dan-jun3 (1.Department of Chemical Engineering,Shaanxi Guofang Institute of Technology,Xian 710300,China,2.West Area Oil Production Company,Yanchang Oil Field CO.,LTD,Yanan 717504,3.College of Chemistry & Chemical Engineering,Yanan University,Yanan 716000,China) |
| Abstract: | Dumbbell-like zinc oxide with sharp tips was prepared by a simple hydrothermal method using zinc nitrate and sodium hydroxide as raw materials,sodium oleate as morphology control agent in alcohol/water solution at 230℃.The structure and morphology of samples were studied by X-ray diffraction（XRD） and scanning electron microscope（SEM）.The growth mechanism of the crystal was also discussed. |
| Keywords: | dumbbell zinc oxide microcrystalline hydrothermal synthesis morphology control agent |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ | |