| 桥链双中环二胺的合成与表征 |
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| 引用本文： | 朱棉霞,王竹梅,展红全. 桥链双中环二胺的合成与表征[J]. 江西师范大学学报(自然科学版), 2007, 31(6): 584-587 |
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| 作者姓名： | 朱棉霞 王竹梅 展红全 |
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| 作者单位： | 景德镇陶瓷学院,材料科学与工程学院,景德镇,333403;景德镇陶瓷学院,材料科学与工程学院,景德镇,333403;景德镇陶瓷学院,材料科学与工程学院,景德镇,333403 |
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| 摘 要： | 以含羟基中环二胺为原料,在氢化钠存在下,与多甘醇二对甲苯酸酯或二溴代烷烃发生偶合,合成了6个新型桥链双中环二胺化合物,并通过核磁共振谱、质谱、元素分析和红外光谱表征了其结构.
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| 关 键 词： | 桥链 中环二胺 偶合 表征 |
| 文章编号： | 1000-5862（2007）06-0584-04 |
| 收稿时间： | 2007-10-09 |
| 修稿时间： | 2007-10-09 |
Synthesis and Characterization of Bridged Double Mesocyclic Diamine |
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| ZHU Mian-xia,WANG Zhu-mei,ZHAN Hong-quan. Synthesis and Characterization of Bridged Double Mesocyclic Diamine[J]. Journal of Jiangxi Normal University (Natural Sciences Edition), 2007, 31(6): 584-587 |
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| Authors: | ZHU Mian-xia WANG Zhu-mei ZHAN Hong-quan |
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| Abstract: | In this paper,by using hydroxyl mesocyclic diamine as raw material,we synthesized six novel compounds of bridged double mesocyclic diamine through the coupling reaction with multi-glycol p-xylene acid ester or dibromoalkane,under the existing of Sodium hydride.And the structure of these products were characterized by nuclear magnetic resonance spectrometry,mass spectrometry,element analysis and infrared spectrum. |
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| Keywords: | bridged double mesocyclic diamine coupling reaction characterization |
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