| 气相色谱法测定轻烃及其产品中的含硫化合物 |
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| 引用本文： | 窦云芹,李晓丽,宋会美,张立超,曹帼英,谷晓庆,张寒琦.气相色谱法测定轻烃及其产品中的含硫化合物[J].吉林大学学报(理学版),2008,46(3):552-555. |
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| 作者姓名： | 窦云芹 李晓丽 宋会美 张立超 曹帼英 谷晓庆 张寒琦 |
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| 作者单位： | 1. 大庆油田化工有限公司技术开发研究院 分析检测中心, 黑龙江 大庆 163453； 2. 吉林大学 化学学院, 长春 130012 |
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| 基金项目： | 国家科技支撑计划
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大庆石油管理局科研项目 |
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| 摘 要： | 利用气相色谱火焰光度检测法测定轻烃及其产品中的含硫化合物, 考察了实验条件, 并研究了适合于测定的各种标准曲线类型. 结果表明, 含2-丙硫醇、 1-丙硫醇和甲硫醚的测定下限分别为0.56,0.21,0.37 mg/L.
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| 关 键 词： | 含硫化合物 轻烃 火焰光度检测器 |
| 文章编号： | 1671-5489(2008)03-0552-04 |
| 收稿时间： | 2007-05-23 |
| 修稿时间： | 2007年5月23日 |
Determination of Sulfur Compounds in Light Hydrocarbon and Its Products by Gas Chromatography |
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| DOU Yun-qin,LI Xiao-li,SONG Hui-mei,ZHANG Li-chao,CAO Guo-ying,GU Xiao-qing,ZHANG Han-qi.Determination of Sulfur Compounds in Light Hydrocarbon and Its Products by Gas Chromatography[J].Journal of Jilin University: Sci Ed,2008,46(3):552-555. |
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| Authors: | DOU Yun-qin LI Xiao-li SONG Hui-mei ZHANG Li-chao CAO Guo-ying GU Xiao-qing ZHANG Han-qi |
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| Institution: | 1. Analytical Center, Research Institute of Technology Development, Chemical Engineering andTechnology Corporation of Daqing Oil Field, Daqing 163453, Heilongjiang Province, China； 2. College of Chemistry, Jilin University, Changchun 130012, China |
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| Abstract: | The sulfur compounds in light hydrocarbon and its products were determined by gas chromatography with a flame photometric detector. The experimental conditions were examined and some types of standard curves were studied in detail. The determination limits of 2-propyl mercapan, 1-propyl merca
pan and methyl thioether are 0.56,0.21 and 0.37 mg/L, respectively. The proposed method was applied to the determination of sulfur compounds in light hydrocarbon and its products and the results obtained are satisfactory. |
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| Keywords: | sulfur compounds light hydrocarbon flame photometric detector |
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