| HPLC法同时测定外感风痧颗粒中4种成分 |
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| 引用本文： | 刘雯1,郭海姣1,刘进宝2,覃洁萍1**,胡华3,黄盛梅1,王先军1. HPLC法同时测定外感风痧颗粒中4种成分[J]. 广西科学, 2019, 26(5): 539-542 |
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| 作者姓名： | 刘雯1 郭海姣1 刘进宝2 覃洁萍1** 胡华3 黄盛梅1 王先军1 |
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| 作者单位： | 广西中医药大学药学院,广西南宁 530001;广西国际壮医医院,广西南宁 530200;广西中医药大学制药厂,广西南宁530023 |
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| 基金项目： | 广西高校中药提取纯化与质量分析重点实验室项目（桂教科研[2014]6）和广西高校壮医方药基础与应用研究重点实验室（厅级）科研课题（桂教科研[2016]6 zyfy201608）资助。 |
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| 摘 要： | 本文建立同时测定外感风痧颗粒中原儿茶酸、原儿茶醛、绿原酸、咖啡酸4种成分的HPLC方法。色谱柱为依利特Hypersil C18柱(250 mm×4.6 mm,5μm);流动相为乙腈-0.2%磷酸,梯度洗脱,流速1.0mL·min~(-1);柱温25℃。结果显示:4种指标成分分离效果良好,原儿茶酸在3.672～33.048μg·mL~(-1)、原儿茶醛在1.236～11.124μg·mL~(-1)、绿原酸在9.2～82.8μg·mL~(-1)、咖啡酸在1.488～13.392μg·mL~(-1)线性关系良好;平均加样回收率均为97.6%～103.3%。本方法准确、灵敏、可靠,重现性较好,可用于外感风痧颗粒的质量控制。
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| 关 键 词： | 外感风痧颗粒 HPLC 原儿茶酸 原儿茶醛 绿原酸 咖啡酸 |
Simultaneous determination of four components in Waiganfengsha granule by HPLC |
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| LIU Wen,GUO Haijiao,LIU Jinbao,QIN Jieping,HU Hu,HUANG Shengmei and WANG Xianjun. Simultaneous determination of four components in Waiganfengsha granule by HPLC[J]. Guangxi Sciences, 2019, 26(5): 539-542 |
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| Authors: | LIU Wen GUO Haijiao LIU Jinbao QIN Jieping HU Hu HUANG Shengmei WANG Xianjun |
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| Affiliation: | College of Pharmacy, Guangxi University of Traditional Chinese Medicine, Nanning, Guangxi, 530001, China,College of Pharmacy, Guangxi University of Traditional Chinese Medicine, Nanning, Guangxi, 530001, China,International Zhuang Medical Hospital of Guangxi, Nanning, Guangxi, 530200, China,College of Pharmacy, Guangxi University of Traditional Chinese Medicine, Nanning, Guangxi, 530001, China,Pharmaceutical Factory, Guangxi University of Chinese Medicine, Nanning, Guangxi, 530023, China,College of Pharmacy, Guangxi University of Traditional Chinese Medicine, Nanning, Guangxi, 530001, China and College of Pharmacy, Guangxi University of Traditional Chinese Medicine, Nanning, Guangxi, 530001, China |
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| Abstract: | |
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| Keywords: | Waiganfengsha granule HPLC protocatechuic acid protocatechuic aldehyde chlorogenic acid caffeic acid |
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