| 海洋中药厚藤的质量标准研究 |
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| 引用本文： | 冯小慧,,,韦棪婷,,,邓家刚,,,谢滟,,,徐炜杰,,,侯小涛,,.海洋中药厚藤的质量标准研究[J].广西科学,2019,26(5):503-510. |
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| 作者姓名： | 冯小慧 韦棪婷 邓家刚 谢滟 徐炜杰 侯小涛 |
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| 作者单位： | 广西中医药大学,广西南宁 530200;广西中药药效研究重点实验室,广西南宁 530200;广西农作物废弃物功能成分研究协同创新中心,广西南宁 530200;广西中医药大学,广西南宁 530200;广西中药药效研究重点实验室,广西南宁 530200;广西农作物废弃物功能成分研究协同创新中心,广西南宁 530200;广西中医药大学,广西南宁 530200;广西中药药效研究重点实验室,广西南宁 530200;广西农作物废弃物功能成分研究协同创新中心,广西南宁 530200;广西中医药大学,广西南宁 530200;广西中药药效研究重点实验室,广西南宁 530200;广西农作物废弃物功能成分研究协同创新中心,广西南宁 530200;广西中医药大学,广西南宁 530200;广西中药药效研究重点实验室,广西南宁 530200;广西农作物废弃物功能成分研究协同创新中心,广西南宁 530200;广西中医药大学,广西南宁 530200;广西中药药效研究重点实验室,广西南宁 530200;广西农作物废弃物功能成分研究协同创新中心,广西南宁 530200 |
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| 基金项目： | 广西科技计划项目（桂科AD17195025）和2018广西一流学科建设项目重点课题（2018XK043）资助。 |
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| 摘 要： | 为了建立海洋中药厚藤(Ipomoea pes-caprae (Linn.)Sweet)的质量标准,本研究采用薄层色谱法,以咖啡酸为对照品,对厚藤进行定性鉴别;采用高效液相色谱法,对厚藤中绿原酸、咖啡酸、异槲皮苷、异绿原酸B、异绿原酸A、异绿原酸C等6个成分进行含量测定。结果显示,本研究建立的厚藤薄层色谱鉴别法,色谱图斑点清晰,分离度好,专属性强;检测得到10批不同产地厚藤中6个成分的含量范围。表明本研究建立的质量标准可有效控制厚藤的质量。
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| 关 键 词： | 厚藤 海洋中药 质量标准 TLC HPLC |
Study on quality standard of traditional marine Chinese medicine Ipomoea pes-caprae |
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| FENG Xiaohui,WEI Yanting,DENG Jiagang,XIE Yan,XU Weijie and HOU Xiaotao.Study on quality standard of traditional marine Chinese medicine Ipomoea pes-caprae[J].Guangxi Sciences,2019,26(5):503-510. |
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| Authors: | FENG Xiaohui WEI Yanting DENG Jiagang XIE Yan XU Weijie and HOU Xiaotao |
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| Institution: | Guangxi University of Chinese Medicine, Nanning, Guangxi, 530200, China;Guangxi Key Laboratory of Efficacy Study on Chinese Materia Medicia, Nanning, Guangxi, 530200, China;Guangxi Collaborative Innovation Center for Research on Functional Ingredients of Agricultural Residues, Nanning, Guangxi, 530200, China,Guangxi University of Chinese Medicine, Nanning, Guangxi, 530200, China;Guangxi Key Laboratory of Efficacy Study on Chinese Materia Medicia, Nanning, Guangxi, 530200, China;Guangxi Collaborative Innovation Center for Research on Functional Ingredients of Agricultural Residues, Nanning, Guangxi, 530200, China,Guangxi University of Chinese Medicine, Nanning, Guangxi, 530200, China;Guangxi Key Laboratory of Efficacy Study on Chinese Materia Medicia, Nanning, Guangxi, 530200, China;Guangxi Collaborative Innovation Center for Research on Functional Ingredients of Agricultural Residues, Nanning, Guangxi, 530200, China,Guangxi University of Chinese Medicine, Nanning, Guangxi, 530200, China;Guangxi Key Laboratory of Efficacy Study on Chinese Materia Medicia, Nanning, Guangxi, 530200, China;Guangxi Collaborative Innovation Center for Research on Functional Ingredients of Agricultural Residues, Nanning, Guangxi, 530200, China,Guangxi University of Chinese Medicine, Nanning, Guangxi, 530200, China;Guangxi Key Laboratory of Efficacy Study on Chinese Materia Medicia, Nanning, Guangxi, 530200, China;Guangxi Collaborative Innovation Center for Research on Functional Ingredients of Agricultural Residues, Nanning, Guangxi, 530200, China and Guangxi University of Chinese Medicine, Nanning, Guangxi, 530200, China;Guangxi Key Laboratory of Efficacy Study on Chinese Materia Medicia, Nanning, Guangxi, 530200, China;Guangxi Collaborative Innovation Center for Research on Functional Ingredients of Agricultural Residues, Nanning, Guangxi, 530200, China |
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| Abstract: | This study was conducted to establish the quality standard of marine Chinese medicine Ipomoea pes-caprae.Ipomoea pes-caprae was identified with caffeic acid as the reference substance by TLC.The content of six components such as caffeic acid,chlorogenic acid,isoquercitrin,isochlorogenic acid B,I sochlorogenic acid A,and isochlorogenic acid C in Ipomea pes-caprae was determined by high performance liquid chromatography.A TLC method for identification of Ipomoea pes-caprae was established.The chromatograms for Ipomoea pes-caprae were clear,the resolution was good,and the specificity was strong.The content range of 6 components in 10 batches of different Ipomoea pes-caprae was detected.The quality standards established in this study can effectively control the quality of Ipomoea pes-caprae. |
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| Keywords: | Ipomoea pes-caprae marine Chinese medicine quality standard TLC HPLC |
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