| 以1,4-二碘丁烷为中间体双螺环螺恶嗪的合成与表征 |
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| 引用本文： | 杨志范,安晶,杨宇明,程伟.以1,4-二碘丁烷为中间体双螺环螺恶嗪的合成与表征[J].吉林工学院学报,2005,26(1):8-10. |
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| 作者姓名： | 杨志范 安晶 杨宇明 程伟 |
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| 作者单位： | 长春工业大学化学工程学院 吉林长春130012
(杨志范，安晶，杨宇明)，长春工业大学化学工程学院 吉林长春130012(程伟) |
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| 基金项目： | 吉林省科技厅应用基础理论资助项目(吉科合字第20010153号) |
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| 摘 要： | 有关螺恶嗪的衍生物的光致变色研究已有多人报道．主要集中在两个方面：一是设计不同的螺恶嗪分子，研究分子结构对光致变色行为的影响；另一方面是探讨介质对光致变色行为的影响。文中以1，4-二碘丁烷为中间体，合成了双螺环螺恶嗪。通过IR,^1HNMR手段进行表征。确认了产物结构。
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| 关 键 词： | 双螺环 螺恶嗪 衍生物 |
| 文章编号： | 1006-2939(2005)01-0008-03 |
The synthesis of bis-spironaphthoxazine using 1,4-diiodobutane as a medium and the characterization of the product |
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| YANG Zhi-fan,AN Jing,YANG Yu-ming,CHENG Wei.The synthesis of bis-spironaphthoxazine using 1,4-diiodobutane as a medium and the characterization of the product[J].Journal of Jilin Institute of Technology,2005,26(1):8-10. |
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| Authors: | YANG Zhi-fan AN Jing YANG Yu-ming CHENG Wei |
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| Abstract: | Among the vast number of reports on the photochrometry of spirooxazine derivatives in the literature, researchers are mainly interested in two aspects: one designs different spirooxazines, and looks into the influence of the structure on the photochromic behaviour; the other inquires into the (influence) of the medium on photochromic behaviour. In this work, 1,4-diiodobutane was used as the medium to synthesize bis-spirnaphthoxazine. The product was identified by elemental analysis, IR and ~1H NMR, and the resultant structure was confirmed. |
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| Keywords: | bis-spironaphthoxazine spirooxazine derivatives |
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