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2,4-二氯苯甲醛在有机溶剂中的溶解度
引用本文:黑恩成,刘洪来,李建军.2,4-二氯苯甲醛在有机溶剂中的溶解度[J].华东理工大学学报(自然科学版),1993(4).
作者姓名:黑恩成  刘洪来  李建军
作者单位:华东化工学院化学系 (黑恩成,刘洪来),华东化工学院化学系(李建军)
摘    要:改进了Proust等测定液-固平衡的装置和方法,并用该装置测定了2,6-二甲基苯酚在环己烷中和2,4-二氟苯甲醛在乙醇、丙酮、乙酸中的溶解度,测温误差为0.04K,液相组成误差为0.000 5。

关 键 词:溶解度  热分析  液-固平衡  2  6-二甲基苯酚  2  4-二氯苯甲醛

Solubility of 2,4-Dichlorobenzaldehyde in Organic Solvent
Hei Encheng,Liu Honglai and Li Jianjun.Solubility of 2,4-Dichlorobenzaldehyde in Organic Solvent[J].Journal of East China University of Science and Technology,1993(4).
Authors:Hei Encheng  Liu Honglai and Li Jianjun
Institution:Department of Chemistry
Abstract:An improved version of the method and instrument of solid-liquid equilibrium has been calibrated. The solubility of 2,6-dimethylphenol in cyclohexane was measured by this equipment and the data agree with literature values. On this basis, the solubilities of 2,4-dichlorobenzaldehyde in ethyl alcohol, acetone, acetic acid were measured accurately and correlated by UNIQUAC activity coefficient model. Those data can be used as the basis of selection of the process parameters in purification and crystallization of 2, 4-dichlorobenzaldehyde.
Keywords:solubility  thermal analysis  solid-liquid equilibria  2  6-dimethylphenol  2  4-dichlorobenzaldehyde  
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