| 六硝基联苄氧化成六硝基芪的研究 |
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| 引用本文： | 陆明.六硝基联苄氧化成六硝基芪的研究[J].南京理工大学学报(自然科学版),1992(4). |
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| 作者姓名： | 陆明 |
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| 作者单位： | 华东工程学院化工学院 |
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| 摘 要： | 该文介绍以六硝基联苄(HNBB)为中间体,用梯恩梯(TNT)为原料,分两步合成六硝基艺(HNS)的工艺路线,给出了六硝基联苄氧化成六硝基(艹氐)的最佳工艺条件。文中详细讨论了反应母液循环套用对六硝基(艹氐)的得率和质量的影响,并用核磁共振谱(NMR)研究了水对反应的影响。
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| 关 键 词： | 炸药 硝基化合物 合成 |
A Study on Hexanitrobibenzil Being Oxidized into Hexanitrostilbene. |
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| Lu Ming Chemical Engineering School.A Study on Hexanitrobibenzil Being Oxidized into Hexanitrostilbene.[J].Journal of Nanjing University of Science and Technology(Nature Science),1992(4). |
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| Authors: | Lu Ming Chemical Engineering School |
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| Institution: | Lu Ming Chemical Engineering School |
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| Abstract: | The technological route of the synthesis of HNS in two steps byraw material TNT through intermediate HNBB is introduced. The best techno-logical condition in which HNBB is oxidized into HNS is given. The effect ofthe reacting solvent reused cyclically on the yield and quality of HNS is dis-cussed. The effect of water on the reaction is studied by NMR. |
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| Keywords: | explosive nitrocompounds syntbesis |
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