| 异长叶烯Prins反应及其产物的分离 |
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| 引用本文： | 余德润,黄晓宾,李冲,阳东青,蒋凤池.异长叶烯Prins反应及其产物的分离[J].江西师范大学学报(自然科学版),2005,29(6):522-524. |
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| 作者姓名： | 余德润 黄晓宾 李冲 阳东青 蒋凤池 |
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| 作者单位： | 江西生物科技职业学院,江西,南昌,330200;江西师范大学,江西,南昌,330027;重庆大学,重庆,400000 |
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| 摘 要： | 探讨了异长叶烯的Prins反应条件及其产物的分离．异长叶烯的Prins反应产物主要有两种，这两种化合物很难分离，该文用柱层析成功地把这两种化合物分离出来，纯度可达97．2％．
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| 关 键 词： | 异长叶烯 Prins反应 柱层析 |
| 文章编号： | 1000-5862（2005）06-0522-03 |
| 收稿时间： | 2005-04-27 |
| 修稿时间： | 2005-04-27 |
The Prins Reaction of Isolongifolene and Separation of Products |
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| YU De-Run,HUANG Xiao-bin,LI Chong,YANG Dong-qing,JIANG Feng-chi.The Prins Reaction of Isolongifolene and Separation of Products[J].Journal of Jiangxi Normal University (Natural Sciences Edition),2005,29(6):522-524. |
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| Authors: | YU De-Run HUANG Xiao-bin LI Chong YANG Dong-qing JIANG Feng-chi |
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| Institution: | 1. Jiangxi Biological Science and Technology Vocational College, Nanchang 330200, China; 2. Jiangxi Normal University Nanchang 330027, China;3. Chongqing University, Chongqing 400000, China |
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| Abstract: | The Prins reaction of isolongifolene give a mixture of 8 - acetexymethylisolongifolene and 8 - acetoxymethylcy - cloisolongifolene as the reaction products. It is very difficult to separate them and they have not been separated easier by column chromatography over silica gel. Now we have successfully separated them by the column chromatography over silica gel ; their pure can reach to 97.2%. |
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| Keywords: | Isolongifolene Prins reaction column chromatography separate 8 - acetexymethylisolongifolene 8 - ace- toxymethylcy - cloisolongifolene |
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