| 气相色谱-卧管式微火焰原子吸收法测定底泥中的二乙基汞 |
| |
| 引用本文： | 孙汉文,孙建民,乔玉卿,阎正.气相色谱-卧管式微火焰原子吸收法测定底泥中的二乙基汞[J].河北大学学报(自然科学版),2000,20(3):252-255. |
| |
| 作者姓名： | 孙汉文 孙建民 乔玉卿 阎正 |
| |
| 作者单位： | 河北大学,化学系,河北,保定,071002 |
| |
| 基金项目： | 河北省教委资助项目(296064) |
| |
| 摘 要： | 介绍了气相色谱 -卧管式微火焰原子吸收联用测定底泥中二乙基汞的新方法 .样品经EDTA处理后 ,以正辛烷萃取 ,离心分离有机相 ,浓缩后直接进样分析 .检出限为3.5×10 -11 g,RSD为1.4 % .
|
| 关 键 词： | 萃取 二乙基汞 正辛烷 底泥 气相色谱-原子吸收联用 |
| 文章编号： | 1000-1565(2000)03-0252-04 |
| 修稿时间： | 2000-01-20 |
Determination of Diethylmercury in Sediment by Gas Chromatography - Atomic Absorption Spectrometry with Horizontal Pipe Mini- Flame Atomizer Equipment |
| |
| SUN Han-wen,SUN Jian-min,QIAO Yu-qing,YAN Zheng.Determination of Diethylmercury in Sediment by Gas Chromatography - Atomic Absorption Spectrometry with Horizontal Pipe Mini- Flame Atomizer Equipment[J].Journal of Hebei University (Natural Science Edition),2000,20(3):252-255. |
| |
| Authors: | SUN Han-wen SUN Jian-min QIAO Yu-qing YAN Zheng |
| |
| Institution: | SUN Han-wen
,SUN Jian-min
,QIAO Yu-qing
,YAN Zheng
;(Department of Chemistry, Hebei University, Baoding 071002, China) |
| |
| Abstract: | A new method has been proposed for the determination of diethylmercury in sediment by gas chromatography -atomic absorption spectrometry with horizontal pipe mini-flame atomizer equipment. The samples treated with EDTA were entracted with n-octane and centrifugalized. The concentrated organic solution was injected into GC-AAS system for analysis. Diethylmercury content in sediment samples was determined satisfacterily with a relative sdandard diviation of 1.4% and a detection limit of 3.5×10-11 g. |
| |
| Keywords: | extraction diethylmercury n-octane sediment GCAAS |
| 本文献已被 CNKI 万方数据 等数据库收录！ |
|
