| 一种合成硫代氨基甲酸酯类化合物的新工艺 |
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| 引用本文： | 刘大勇,牛建兵,赵丽娜.一种合成硫代氨基甲酸酯类化合物的新工艺[J].江西师范大学学报(自然科学版),2007,31(6):566-569. |
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| 作者姓名： | 刘大勇 牛建兵 赵丽娜 |
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| 作者单位： | 黄淮学院,化学化工系,河南,驻马店,463000 |
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| 基金项目： | 河南省科技攻关课题资助项目(0624270024) |
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| 摘 要： | 阐述了一种用易得的原料苯胺和硫醇等"一锅法"合成硫代氨基甲酸酯类化合物的新工艺,该工艺催化剂价廉易得、催化活性高,且易于分离、回收,并能循环使用;反应步骤短,操作简单,有利于大规模工业化生产;避免了光气的使用,且反应无需溶剂,副产物是水,提高了环境友好性.
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| 关 键 词： | 硒 苯胺 硫醇 硫代氨基甲酸酯类 |
| 文章编号： | 1000-5862（2007）06-0566-04 |
| 收稿时间： | 2007-08-01 |
| 修稿时间： | 2007年8月1日 |
The New Technology about Synthetic Thionocarbamates Compounds |
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| LIU Da-yong,NIU Jian-bin,ZHAO Li-na.The New Technology about Synthetic Thionocarbamates Compounds[J].Journal of Jiangxi Normal University (Natural Sciences Edition),2007,31(6):566-569. |
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| Authors: | LIU Da-yong NIU Jian-bin ZHAO Li-na |
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| Abstract: | The latest technology-pot making was described that using a readily available materials,such as aniline and mercaptan,synthesized thionocarbamates compounds.This process catalyst was cheap,easy and getting high catalytic activity.Even more,it could be easily separated,recycled,and reused.Short reaction steps and simple operation were conducive to large-scale industrial production,avoid the use of phosgene,and no solvent reaction,by-product was water,these improve the environment-friendly.It is the new method of very promising synthetic thionocarbamates. |
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| Keywords: | selenium aniline thiol thionocarbamates |
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