| 硫脲基和席夫碱基取代的硫杂杯[4]芳烃的设计与合成 |
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| 引用本文： | 唐富胜,杨发福,殷凤菊,刘朝晖. 硫脲基和席夫碱基取代的硫杂杯[4]芳烃的设计与合成[J]. 福建师范大学学报(自然科学版), 2008, 24(5) |
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| 作者姓名： | 唐富胜 杨发福 殷凤菊 刘朝晖 |
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| 作者单位： | 福建师范大学化学与材料学院,福建,福州,350108 |
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| 基金项目： | 国家自然科学基金，福建省自然科学基金 |
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| 摘 要： | 对叔丁基硫杂杯[4]芳烃-1,3-二醛基衍生物与苯基氨基硫脲发生"1 2"缩合反应,合成了含硫脲基和席夫碱基的新型硫杂杯[4]芳烃衍生物,后处理简单,产率达85%.新化合物的结构经元素分析、1H NMR和ESI-MS等表征证实.
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| 关 键 词： | 硫杂杯[4]芳烃 席夫碱 硫脲 合成 |
Design and Synthesis of Thiacalix[4]arene Derivative Containing Thiourea and Schiff-base Units |
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| TANG Fu-sheng,YANG Fa-fu,YIN Fengju,LIU Chao-hui. Design and Synthesis of Thiacalix[4]arene Derivative Containing Thiourea and Schiff-base Units[J]. Journal of Fujian Teachers University(Natural Science), 2008, 24(5) |
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| Authors: | TANG Fu-sheng YANG Fa-fu YIN Fengju LIU Chao-hui |
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| Abstract: | By reacting thiacalix[4]arene-1,3-dial derivative with phenyl-thiosemicarbazide in "1 2" condensation,a novel thiacalix[4]arene derivative containing Schiff-base and thiourea units was prepared with simple procedure.The yield was as high as 85%.The structure of new compound was characterized by elemental analysis,1H NMR and ESI-MS,etc. |
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| Keywords: | thiacalix[4]arene Schiff-base thiourea synthesis |
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