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The synthesis of a new type of calix[4]arene with chiral pendant
Authors:He Yong-bing  Li Jian-feng  Meng Ling-zhi  Xiao Yuan-jing  Yu Tian-xiang  Wu Cheng-tai
Institution:(1) College of Chemistry and Molecule Science, Wuhan University, 430072 Wuhan, China
Abstract:Two new chiral calixarenes were synthesized by condensing 1,3-bis-chlorocarbomethyl-calix4] arenes with (1S, 2S)-2-amino-1-(4-nitrophenyl)-1,3-propanediol, a by-product from antibiotic industry, and were characterized by1H-NMR, MS-FAB, and elemental analysis. The1H-NMR spectra show that those molecules assume a cone conformation in solution. Foundation item: Supported by the Zi-Qiang Science Foundation of Wuhan University Biography: He Yong-bing, (1945-), male, Professor, research direction: supramolecular chemistry.
Keywords:Calix[4]arene  chirality  synthesis  conformation
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