| ICP—arc粉末法同时测定有机物中微量元素 |
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| 引用本文： | 谢国勋 林添明. ICP—arc粉末法同时测定有机物中微量元素[J]. 厦门大学学报(自然科学版), 1992, 31(5): 569-571 |
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| 作者姓名： | 谢国勋 林添明 |
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| 作者单位： | 厦门大学化学系(谢国勋，林添明，李文捷，郭文雷)，厦门大学化学系(颜长明) |
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| 摘 要： | ICP光源已广泛和成功地应用于溶液样品的分析。由于固体样品的溶解处理麻烦,溶液进样技术又存在着易沾污和样品被稀释等局限性,所以本实验室致力于固体粉末直接进样法研究,设计了粉末进作器和封闭式ICP-arc加长炬管系统,简称ICP-arc。利用这些装置,可使
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| 关 键 词： | JCP－arc 粉末法 有机物 微量元素 |
The Determination of Trace Elements in Organic Matters by Introducing Powered Sample into ICP-arc |
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| Xie Guoxun Lin Tianming Li Wenjie Guo Wenlei Yan Changming. The Determination of Trace Elements in Organic Matters by Introducing Powered Sample into ICP-arc[J]. Journal of Xiamen University(Natural Science), 1992, 31(5): 569-571 |
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| Authors: | Xie Guoxun Lin Tianming Li Wenjie Guo Wenlei Yan Changming |
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| Affiliation: | Dept. of Chem. |
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| Abstract: | A method for the simultaneous determination of Mn, Fe, Cr, Ni and Cu in organic matters with a powder introduction ICP-arc system has been developed. The results of analysis for the organic samples agree well with certified values. The RSD% are between 6. 03-13. 2% (n = 10) and the recovery ratios are between 95-115% for different elements. Using present method, the concentrations of all elements being determined in the sample are concentrated about 10-20 times. So it is extremely favorable when the quantity of the sample is small and/or the concentration of the element to be determined is low. This method offsets the effects of matrix, particle size and present form of the element on line intensity. It has lower detection limits. |
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| Keywords: | Powder introduction Organic matters analysis ICP-arc |
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