| 3,9-二乙酰基-N-乙基咔唑的合成工艺研究 |
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| 引用本文： | 邓崇海,丁明,王章彪,陈虹.3,9-二乙酰基-N-乙基咔唑的合成工艺研究[J].合肥学院学报(自然科学版),2004,14(1):48-49. |
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| 作者姓名： | 邓崇海 丁明 王章彪 陈虹 |
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| 作者单位： | 合肥学院,安徽,合肥,230022;合肥学院,安徽,合肥,230022;合肥学院,安徽,合肥,230022;合肥学院,安徽,合肥,230022 |
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| 基金项目： | 合肥学院科研项目(代码:521) |
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| 摘 要： | 强双光子技术在未来研究领域中具有强大的应用潜力,合成出新化合物3,9-二乙酰基-N-乙基咔唑,该化合物具有较大双光子吸收截面和强双光子性质,通过采用四因素三水平正交试验,得出最佳的工艺合成条件,放大10倍投料,计算收率为93.2％。
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| 关 键 词： | 3 9-二乙酰基-N-乙基咔唑 合成工艺 正交试验 |
| 文章编号： | 1008-6056(2004)01-0048-02 |
| 修稿时间： | 2004年1月12日 |
Research on Synthetic Technique of the Compound 3,9-biacetyl-N-ethyl Carbazole |
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| DENG Chong-hai,DING Ming,WANG Zhang-biao,CHEN Hong.Research on Synthetic Technique of the Compound 3,9-biacetyl-N-ethyl Carbazole[J].Journal of Hefei University :Natural Sciences,2004,14(1):48-49. |
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| Authors: | DENG Chong-hai DING Ming WANG Zhang-biao CHEN Hong |
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| Abstract: | Strong two-photon technique will have potential application in the future. In this paper, we synthesize a new compound-3, 9-biacetyl-N-ethyl carbazole with large two-photon absorption cross-section for the first time, which have the characteristic of strong two-photon absorption. The optimal technique conditions are achieved by carrying out orthogonal experiments of four factors and three levels. By enlarging 10 times of reactants, the yield is about 93.2%. |
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| Keywords: | 3 9-biacetyl-N-ethyl carbazole synthetic technique orthogonal experiment |
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