| 新型三氮唑吡啶盐负载的脯氨酸手性离子液体的合成和表征 |
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| 引用本文： | 于雅琴. 新型三氮唑吡啶盐负载的脯氨酸手性离子液体的合成和表征[J]. 天津师范大学学报(自然科学版), 2009, 29(4): 47-49 |
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| 作者姓名： | 于雅琴 |
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| 作者单位： | 天津师范大学,水环境与水资源重点实验室,天津,300387 |
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| 基金项目： | 天津市科技发展计划项目,天津师范大学青年基金资助项目 |
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| 摘 要： | 以脯氨酸和吡啶为起始原料,经多步中间体合成了新型三氮唑吡啶盐负载的脯氨酸手性离子液体,并对各中间体与目标化合物的结构进行了核磁共振、元素分析、高分辨质谱和熔点测定的表征.实验结果表明,各中间体及最终产物的产率为71%~88%.
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| 关 键 词： | 脯氨酸 吡啶 离子液体 绿色化学 合成 |
Synthesis and characterization of novel ionic liquid pyrrolidine-based chiral triazole pyridinium |
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| YU Yaqin. Synthesis and characterization of novel ionic liquid pyrrolidine-based chiral triazole pyridinium[J]. Journal of Tianjin Normal University(Natural Science Edition), 2009, 29(4): 47-49 |
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| Authors: | YU Yaqin |
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| Affiliation: | YU Yaqin (Key Laboratory of Water Environment and Water Resource, Tianjin Normal University, Tianjin 300387, China) |
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| Abstract: | Pyrrolidine-based chiral triazole pyridinium ionic liquid has been synthesized with proline and pyridine as original reactants through polystep reactions, and the reaction product has been characterized by ^1H-NMR analysis, elementary analyses, HRMS analysis, and melting point test. The yields of the related intermediates and the target product are 71%-88%. |
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| Keywords: | proline pyridine ionic liquid green chemistry synthesis |
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