| 苯基羟胺及N-酰基衍生物的合成与表征 |
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| 引用本文： | 付时雨,詹怀宇,余惠生. 苯基羟胺及N-酰基衍生物的合成与表征[J]. 华南理工大学学报(自然科学版), 2000, 28(5): 59-63 |
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| 作者姓名： | 付时雨 詹怀宇 余惠生 |
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| 作者单位： | 华南理工大学制浆造纸工程国家重点实验室!广东广州510640(付时雨，詹怀宇)，中国科学院广州化学研究所纤维素化学开放实验室!广东广州510650(余惠生) |
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| 基金项目： | 国家自然科学基金资助项目 !(2 9770 10 )，广东省自然科学基金资助项目 !(970 4 97) |
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| 摘 要： | 以硝基苯为原料在弱酸性条件下，利用锌粉还原合成苯基羟胺，讨论了反应温度对产物得率的影响；在酰卤试剂作用下生成Ｎ－酰化苯基羟胺，并用ＦＴＩＲ和＾１Ｈ－ＮＭＲ表征合成产物苯基羟胺及其衍生物。
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| 关 键 词： | 苯基羟胺 N－酰基衍生物 合成 表征 |
| 修稿时间： | 1999-05-05 |
Synthesis and Characterization of N-Hydroxybenzenamine and Its N-Acylation |
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| FU Shi_yu ,,ZHAN Huan_yu ,YU Hui_sheng. Synthesis and Characterization of N-Hydroxybenzenamine and Its N-Acylation[J]. Journal of South China University of Technology(Natural Science Edition), 2000, 28(5): 59-63 |
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| Authors: | FU Shi_yu ZHAN Huan_yu YU Hui_sheng |
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| Affiliation: | FU Shi_yu 1,2,ZHAN Huan_yu 1,YU Hui_sheng 2 |
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| Abstract: | N_Hydroxybenzenamine was synthesized by reducing nitrobenzene using Zn under weak acidic conditions. The influence of temperature on the yield of the products was discussed. The products synthesized were characterized by FTIR and 1 H_NMR spectroscopy. N_acetyl_hydroxybenzenamine and N_benzoylhydroxybenzenamine were synthesized by the reaction of hydroxybenzenamine with acetyl chloride and benzoyl chloride respectively. |
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| Keywords: | N_Hydroxybenzenamine N_acylation synthesis characterization |
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