Mit Sorptionsmitteln gefüllte Papiere als Dünnschicht-Fertigplatten |
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Authors: | K Figge |
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Institution: | (1) Unilever Forschungslaboratorium, 2 Hamburg 50, Deutschland |
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Abstract: | Summary Paper loses the properties required for use in partition chromatography with increasing degree of grinding of the cellulose from which the paper is made. For example, paper made from a cellulose mixture consisting of 80% (by weight) Aspa-Birkesulfat and 20% Fichtesulfit adsorbs water to a height of 10 cm after 15 min in the case of a degree of grinding of 14.8°SR (Schoppe-Riegler value) and to a height of only 0.9 cm in the case of a value of 73.3°SR. By adding 50–65% (by weight — based on paper) of adsorbents such as Kieselgel G, Kieselgur G, a mixture of both, Aluminiumoxid G and pure silica gel to the finely ground cellulose mixture in the paper-making process, papers are obtained which adsorb water to a height of 7.6 to 9.3 cm. These filled papers are well suited as thin-layer chromatography plates for adsorption chromatography, as was shown by comparative trials with conventional plates using optical brighteners and 2 solvent systems.
Herrn Dr.E. Becker zum 65. Geburtstag gewidmet. |
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