| 微波辐射对甲苯磺酸/C催化合成氯乙酸异丙酯 |
| |
| 引用本文： | 裴蕾.微波辐射对甲苯磺酸/C催化合成氯乙酸异丙酯[J].合肥工业大学学报(自然科学版),2009,32(3). |
| |
| 作者姓名： | 裴蕾 |
| |
| 作者单位： | 哈尔滨理工大学,化学与环境工程学院,黑龙江,哈尔滨,150060 |
| |
| 摘 要： | 文章研究了活性炭固载对甲苯磺酸作催化剂,酸醇摩尔比为1:1.6,环己烷作为带水剂,在160 W功率的微波辐射下回流分水,合成氯乙酸异丙酯.结果表明,所得产品具有很高纯度和收率,克服了传统有机反应时间长、副反应多、产率低及纯度不高的缺点,同时也为其他氯乙酸酯的合成研究提供了发展新空间.
|
| 关 键 词： | 微波辐射 氯乙酸异丙酯 对甲苯磺酸 |
Microwave radiation for synthesis of isopropyl chloroacetate with PTSA/C as the catalyst |
| |
| PEI Lei.Microwave radiation for synthesis of isopropyl chloroacetate with PTSA/C as the catalyst[J].Journal of Hefei University of Technology(Natural Science),2009,32(3). |
| |
| Authors: | PEI Lei |
| |
| Institution: | College of Chemistry and Enviornmental Engineering;Harbin University of Science and Technology;Harbin 150060;China |
| |
| Abstract: | |
| |
| Keywords: | microwave irradiation isopropyl chloroacetate p-toluenesulfonic acid |
| 本文献已被 CNKI 万方数据 等数据库收录！ |
|
