| 多聚金属离子插层Ni-Ti-LDHs的制备与性质 |
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| 引用本文： | 高伟,何杰.多聚金属离子插层Ni-Ti-LDHs的制备与性质[J].安徽理工大学学报(自然科学版),2011,31(1):8-12. |
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| 作者姓名： | 高伟 何杰 |
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| 作者单位： | 安徽理工大学化学工程学院,安徽,淮南,232001 |
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| 基金项目： | 安徽省自然科学基金资助项目，安徽省高校省级自然科学研究重点资助项目 |
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| 摘 要： | 以三乙醇胺(TEA)为抑制剂,采用共沉淀法制备镍钛双金属氢氧化物(Ni-Ti-LDHs),通过离子交换法制备MoO42-和H3Nb6O195-插层化合物,改变材料物理化学性质.采用X射线衍射(XRD)、红外光谱(FT-IR)、扫描电镜(SEM)、透射电镜(TEM)和热重及差热分析(TG-DTA)等方法对插层柱撑化合物及...
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| 关 键 词： | 层状双金属氢氧化物 阴离子交换 钼酸盐 铌酸盐 插层 |
Preparation and Properties of Ni-Ti-LDHs and Their Complexes with POMs |
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| GAO Wei,HE Jie.Preparation and Properties of Ni-Ti-LDHs and Their Complexes with POMs[J].Journal of Anhui University of Science and Technology:Natural Science,2011,31(1):8-12. |
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| Authors: | GAO Wei HE Jie |
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| Institution: | GAO Wei,HE Jie(School of Chemical Engineering,Anhui University of Science and Technology,Huainan Anhui 232001,China) |
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| Abstract: | Polyanions of transition metal(POMs) MoO2-4 and H3Nb6O5-19 intercalated Ni-Ti layered double hydroxides,which was prepared by co-precipitation method with triethanolamine(TEA) as the inhibitor,then alter the physical-chemical properties of materials.The materials as-prepared were characterized by means of power X-ray diffraction(XRD),Fourier transform infrared(FT-IR) Spectroscopy,Scanning electron microscope(SEM),Transmission electron microscopy(TEM) and Thermogravimetry and Differential Thermal Analysis(TG... |
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| Keywords: | Layered double hydroxide Anion-exchange molybdate niobate intercalation |
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