| TS—1分子筛的合成条件和催化反应性能的研究 |
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| 引用本文： | 高铁男,魏荣宝,梁娅,卢世荣,韩宝成,刘述全,殷蕴婷,王旭. TS—1分子筛的合成条件和催化反应性能的研究[J]. 天津理工大学学报, 1998, 0(4) |
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| 作者姓名： | 高铁男 魏荣宝 梁娅 卢世荣 韩宝成 刘述全 殷蕴婷 王旭 |
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| 作者单位： | 天津理工学院化工系!天津,300191(高铁男,魏荣宝,梁娅,卢世荣,韩宝成),南开大学催化剂厂!天津,300071(刘述全,殷蕴婷,王旭) |
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| 基金项目： | 天津市自然科学基金!963605011 |
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| 摘 要： | 用硅胶（或硅溶胶）和钛酸酯在四乙基氢氧化铵（TEAOH）和四下基氢氧化铵（TBAOH）为摸板剂的条件下制备出钛硅分子筛TS—1;骨架红外（IR）、紫外没反射（DRS）、电子能谱（XPS）等,测试结果证实钛进入分子筛骨架;讨论了合成分子筛的条件对分子筛催化性能的影响．
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| 关 键 词： | TS—1分子筛 硅胶 表征 苯酚羟基化 |
Synthetic Conditions and Catalytic Properties of TS-1 Zeolites |
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| Gao Tienan,Wei Rongbao,Liang Ya,Lu shirong,Han Baocheng. Synthetic Conditions and Catalytic Properties of TS-1 Zeolites[J]. Journal of Tianjin University of Technology, 1998, 0(4) |
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| Authors: | Gao Tienan Wei Rongbao Liang Ya Lu shirong Han Baocheng |
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| Abstract: | TS-1 zeolites have been synthesized by silica gel and titanate in the presence of TEAOH and TBAOH. It has been proved that Ti is located in the molecular sieve framework by the framework IR spectra, the diffuse reflectance spectra in the UV-VIS region and XPS technique. The influence of synthetic conditions and catalytic propreties are discussed. |
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| Keywords: | TS-1 zeolites silica gel synthesis characterization hydroxylation of Phenol |
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