| 4,4'-二(烷/芳氧基甲基)联苯的合成 |
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| 引用本文： | 何海鸥,杨雪艳,吴范宏.4,4'-二(烷/芳氧基甲基)联苯的合成[J].华东理工大学学报(自然科学版),2011,37(3):305-310. |
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| 作者姓名： | 何海鸥 杨雪艳 吴范宏 |
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| 作者单位： | 华东理工大学化学与分子工程学院,上海,200237 |
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| 摘 要： | 以4,4'-二氯甲基联苯(4,4'bis(chloromethye)-biphenye,BCMB)为原料,通过Wil-liamson醚合成法制备了一系列4,4'-二(烷/芳氧基甲基)联苯.对化合物4,4'-二(甲氧基甲基)联苯、4,4'-二(丁氧基甲基)联苯以及4,4'-二(苯氧基甲基)联苯的合成工艺进行改进,缩短了反...
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| 关 键 词： | 4 4'-二氯甲基联苯 Williamson醚合成法 4 4'-二(烷/芳氧基甲基)联苯 |
Synthesis of 4,4'-Bis(alkoxy/phenoxy-methyl biphenyl) |
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| HE Hai-ou,YANG Xue-yan,WU Fan-hong.Synthesis of 4,4'-Bis(alkoxy/phenoxy-methyl biphenyl)[J].Journal of East China University of Science and Technology,2011,37(3):305-310. |
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| Authors: | HE Hai-ou YANG Xue-yan WU Fan-hong |
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| Institution: | HE Hai-ou,YANG Xue-yan,WU Fan-hong(School of Chemistry and Molecular Engineering,East China University ofScience and Technology,Shanghai 200237,China) |
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| Abstract: | A series of 4,4'-bis(alkyloxy/phenoxy methyl biphenyl)were synthesized,using 4,4'-bis(chloromethyl)-biphenyl(BCMB) as raw material by Williamson ether synthesis methods.The synthesis process of 4,4'-bis(methoxymethyl) biphenyl,4,4'-bis(butoxymethyl) biphenyl and 4,4'-bis(phenoxymethyl)biphenyl was improved in reaction time and yield.On the basis,a series of new compounds were prepared. |
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| Keywords: | 4 4'-bis(chloromethyl)biphenyl Williamson ether synthesis 4'-bis(alkoxy/phenoxy-methyl biphenyl) |
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