| 3-氟-4-甲苯腈的合成 |
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| 引用本文： | 刘民.3-氟-4-甲苯腈的合成[J].渤海大学学报(自然科学版),2006,27(3):209-211. |
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| 作者姓名： | 刘民 |
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| 作者单位： | 辽宁工程技术大学,基础科学部,辽宁,阜新,123000 |
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| 摘 要： | 以邻甲基苯胺为原料，经硝化、重氮化、氟化、还原、氧化等反应，成功合成了3-氟-4-甲基苯腈。检索文献国内、国外尚无报道。此工艺路线易控制，收率可达48％，产品纯度高。此产品的研究对于新型农药的开发与生产具有现实的、重要的指导意义。
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| 关 键 词： | 氟化 氰化 3-氟-4甲基苯腈 合成 |
| 文章编号： | 1673-0569(2006)03-0209-03 |
| 收稿时间： | 06 12 2006 12:00AM |
| 修稿时间： | 2006年6月12日 |
Synthesize 3-fluoro-4-methylbenzonitrile |
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| LIU Min.Synthesize 3-fluoro-4-methylbenzonitrile[J].Journal of Bohai University:Natural Science Edition,2006,27(3):209-211. |
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| Authors: | LIU Min |
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| Institution: | Basic Science Institute ,University of Engineering Technology,Fuxin 123000,China |
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| Abstract: | By using ortho-toluidine as a raw material,3-fluoro-4-methylbenzonitrile is successfully synthesized by going through nitrification,diazotization,fluorination,reductive and oxidation reactions.This result hasn't been repothedly achieved both at home and abroad.This kind of production is easy to control and the successful productivity is 48%.The final product is of great practical importance to the development and production of new pesticides. |
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| Keywords: | flurization cyanidation 3-fluoro-4-methylbenzonitrile syntheization |
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