| 3－乙酰基酚酮与TMB等芳醛缩合反应的研究 |
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| 引用本文： | 张宝田,高文涛,付德才. 3－乙酰基酚酮与TMB等芳醛缩合反应的研究[J]. 首都师范大学学报(自然科学版), 1994, 0(4) |
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| 作者姓名： | 张宝田 高文涛 付德才 |
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| 作者单位： | 锦州师范学院化学系，河北轻化工学院 |
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| 摘 要： | 本文探讨了３－乙酰基酚酮与ＴＭＢ等芳香醛的羟醛缩合反应．３－乙酰基酚酮与ＴＭＢ、丁香醛、胡椒醛等取代醛反应分别生成３－［３，４，５－三甲氧基］肉桂酰基酚酮、３－［４－羟基－３，５－二甲氧基］肉桂酰基酚酮、３－［３，４－亚甲二氧基］肉桂酰基酚酮，与桂皮醛反应生成３－［５－苯基－２，４－戊二烯酰基］酚酮等四种新化合物．其结构经红外光谱、核磁共振谱及元素分析得以证实
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| 关 键 词： | 3－乙酰基 酚酮，TMB，缩合反应 |
Condensation Reaction of 3-Acetyltropolone with Aromatic Aldehydes(TMB) |
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| Zhang Baotian,Gao Wentao. Condensation Reaction of 3-Acetyltropolone with Aromatic Aldehydes(TMB)[J]. Journal of Capital Normal University(Natural Science Edition), 1994, 0(4) |
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| Authors: | Zhang Baotian Gao Wentao |
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| Abstract: | Four new products are obtained by aldol condensation reaction of 3-acetyltropolone with aromatic aldehydes such as 3,4,5-trimethoxybenzaldehyde,3,4-methylenezaldehyde,4-hydroxy-3,5-dimethoxybenzaldehyde and cinnamaldehyde in the presence of KOH.Their structures are confirmed by their IR,H-NMR spectral and elementary analysis. |
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| Keywords: | acetyltropolone aromatic aldehyde condensation reaction |
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