| 二氯乙酰氯合成方法的探讨 |
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| 引用本文： | 黄锦霞.二氯乙酰氯合成方法的探讨[J].湖北大学学报(自然科学版),1988(3). |
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| 作者姓名： | 黄锦霞 |
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| 作者单位： | 湖北大学化学系 |
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| 摘 要： | 本文对比了二氯乙酰氯不同制备方法的优缺点,着重对三氯乙烯氧化法进行了较系统的研究,考察了影响三氯乙烯转化率的各种因素。测试数据显示了反应过程中各化学成分及其比例的变化规律。本合成法步骤短,工艺简单,二氯乙酰氯收率达到89％,明显优于其他方法。
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| 关 键 词： | 二氯乙酰氯 三氯乙烯 氧化法 |
STUDY ON SYNTHETIC METHODS OF DICHLOROACETYL CHLORIDE |
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| Huang Jinxia.STUDY ON SYNTHETIC METHODS OF DICHLOROACETYL CHLORIDE[J].Journal of Hubei University(Natural Science Edition),1988(3). |
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| Authors: | Huang Jinxia |
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| Institution: | Department of Chemistry |
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| Abstract: | This paper studid on Synthetic methods of dichloroacetyl Chloride. Dichloroacetyl Chloride was prepared by oxidizing trichloroethylene with oxygen in a yield of 89%. Various factors, Such as the amount of catalysts, the time and the pre ssure of reaction, havev been studied. The results Showed that this process, as compared with the others, has many advantages. |
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| Keywords: | Dichloroacetyl Chloride Trichloroethylene Oxygen m-tehod |
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