| 纤维素在NaOH/尿素/硫脲复合溶剂体系中的溶解性能研究 |
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| 引用本文： | 李荣超,郭宪英.纤维素在NaOH/尿素/硫脲复合溶剂体系中的溶解性能研究[J].科学技术与工程,2011,11(10). |
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| 作者姓名： | 李荣超 郭宪英 |
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| 作者单位： | 青岛大学化学化工与环境学院,青岛,266071 |
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| 摘 要： | 纤维素可溶于NaOH/尿素/硫脲复合溶剂体系.实验采用正交实验的方法研究了NaOH/尿素/硫脲的浓度对纤维素溶解的影响,以及各种溶解条件对溶解效果的影响.通过用XRD、FT-IR表征了该体系下所得的再生纤维素膜.结果表明:纤维素在该水溶液体系下的最佳溶解条件:NaOH的质量分数7%,尿素的质量分数7%,硫脲的质量分数10%,冷冻温度-10℃,在该条件下对纤维素有很好的溶解性能且纤维素溶解再生后为纤维素Ⅱ.
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| 关 键 词： | 纤维素 正交试验 再生纤维素膜 |
| 收稿时间： | 1/4/2011 1:40:07 PM |
| 修稿时间： | 1/12/2011 1:55:14 PM |
Study the performance of Cellulose dissolution in NaOH/urea/thiourea compound resolver system |
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| lirongchao and guoxianying.Study the performance of Cellulose dissolution in NaOH/urea/thiourea compound resolver system[J].Science Technology and Engineering,2011,11(10). |
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| Authors: | lirongchao and guoxianying |
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| Institution: | College of Chemical and Environmental Engineering, Qingdao University |
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| Abstract: | The cellulose may dissolve in the NaOH/urea/thiourea compound resolver system.This experiment used the orthogonal experiment's method study the NaOH/urea/thiourea density the influence which dissolved to the cellulose,and the influence of each kind of dissolved condition to the dissolves effect,XRD,FT-IR are used to attribute under this system the obtained regenerated cellulose membrane.The results indicate that,the best dissolved condition of cellulose under this system is NaOH/urea/thiourea/water quality score 7/7/10/76 and chilling point -10℃.Under this condition is known as the very good dissolved performance and the cellulose dissolution regeneration fiber membrane is the cellulose Ⅱ. |
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| Keywords: | cellulose orthogonal experiment regeneration fiber membrane |
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