| 微波辐射下用高铁酸钾选择氧化苯甲醇合成苯甲醛 |
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| 引用本文： | 李青,刘耀华. 微波辐射下用高铁酸钾选择氧化苯甲醇合成苯甲醛[J]. 太原师范学院学报(自然科学版), 2011, 10(3): 99-100,151 |
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| 作者姓名： | 李青 刘耀华 |
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| 作者单位： | 太原师范学院化学系,山西太原,030031 |
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| 基金项目： | 山西省教育厅科技研究开发项目资助课题(20081039) |
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| 摘 要： | 研究微波辐射条件下高铁酸钾选择氧化苯甲醇合成苯甲醛.结果表明:环己烷和氢氧化钠水溶(pH=11.5)作溶剂,三乙基苄基氯化铵作相转移溶剂,微波功率240W,高铁酸钾氧化苯甲醇合成苯甲醛,产率可达89%.
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| 关 键 词： | 苯甲醇 苯甲醛 相转移溶剂 绿色合成 微波 |
Synthesis of Benzaldehyde from Benzyl Alcohol by Selective Oxidation with Potassium Ferrate in Microwave Radiation |
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| Li Qing Liu Yaohua. Synthesis of Benzaldehyde from Benzyl Alcohol by Selective Oxidation with Potassium Ferrate in Microwave Radiation[J]. Journal of Taiyuan Normal University:Natural Science Edition, 2011, 10(3): 99-100,151 |
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| Authors: | Li Qing Liu Yaohua |
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| Affiliation: | Li Qing Liu Yaohua(Department of Chemistry,Taiyuan Normal University,Taiyuan 030031,China) |
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| Abstract: | In microwave radiation condition,the result of benzyl alcohol by selective oxidation with potassium ferrate in cyclohexane and aqueous solution of sodium hydroxide(pH=11.5) contained phase transfer catalyst indicated that the benzyl alcohol receiving rate above 89%. |
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| Keywords: | benzyl alcohol benzaldehyde phase transfer solvent green synthesis microwave |
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