| Ni2+/纳米MoS2插层化合物的制备及催化性能表征 |
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| 引用本文： | 胡承诚,胡坤宏,程亚洲,徐玉福,胡献国.Ni2+/纳米MoS2插层化合物的制备及催化性能表征[J].合肥工业大学学报(自然科学版),2011(10):1555-1557. |
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| 作者姓名： | 胡承诚 胡坤宏 程亚洲 徐玉福 胡献国 |
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| 作者单位： | 合肥工业大学化学工程学院;合肥工业大学机械与汽车工程学院; |
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| 摘 要： | 文章分别采用市售微米MoS2和自制纳米MoS2作为原料,通过剥层法合成了单层MoS2悬浮液.在2种单层MoS2悬浮液中分别加入等量硫酸镍溶液,调节pH值使单层MoS2发生重堆积反应,可得到Ni2+/微米MoS2和Ni2+/纳米MoS2插层化合物.利用X射线衍射仪、扫描电镜和原子吸收光谱仪对插层化合物进行表征,并考察了2...
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| 关 键 词： | 二硫化钼 插层化合物 催化氧化 |
Synthesis and catalytic properties of Ni~(2+)/nano-MoS_2 intercalation compounds |
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| HU Cheng-cheng,HU Kun-hong,CHENG Ya-zhou,XU Yu-fu,HU Xian-guo.Synthesis and catalytic properties of Ni~(2+)/nano-MoS_2 intercalation compounds[J].Journal of Hefei University of Technology(Natural Science),2011(10):1555-1557. |
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| Authors: | HU Cheng-cheng HU Kun-hong CHENG Ya-zhou XU Yu-fu HU Xian-guo |
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| Institution: | HU Cheng-cheng1,2,HU Kun-hong2,CHENG Ya-zhou1,XU Yu-fu2,HU Xian-guo2(1.School of Chemical Engineering,Hefei University of Technology,Hefei 230009,China,2.School of Machinery and Automobile Engineering,China) |
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| Abstract: | Two monolayer MoS2 suspensions were respectively synthesized from commercial micro-MoS2 and self-made nano-MoS2 by an exfoliation method.The two suspensions were restacked by adjusting pH value in a NiSO4 solution,leading to Ni2+/micro-MoS2 and Ni2+/nano-MoS2 intercalation compounds.The obtained two intercalation compounds were characterized by using the X-ray diffractometer,scanning electron microscope and atomic absorption spectrophotometer respectively.Their catalytic properties were also investigated by... |
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| Keywords: | molybdenum disulfide(MoS2) intercalation compound catalytic oxidation |
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