| 红景天苷合成工艺 |
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| 引用本文： | 徐利锋,曹 迪,姜 帆,李 萌,宁宝入,宋 洋,王 琦,倪 晋,周云鹏,王 洋.红景天苷合成工艺[J].辽宁大学学报(自然科学版),2014(1):71-75. |
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| 作者姓名： | 徐利锋 曹 迪 姜 帆 李 萌 宁宝入 宋 洋 王 琦 倪 晋 周云鹏 王 洋 |
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| 作者单位： | 辽宁大学药学院,辽宁沈阳110036 |
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| 摘 要： | 目的:降低红景天苷的制备成本并且提高红景天苷的产率,研究红景天苷合成的新工艺.方法:本实验以对羟基苯乙醇为原料,通过与糖苷化反应得到红景天苷化合物.结果:经高效液相色谱(HPLC)检测得到的红景天苷单体纯度达到98.5%以上,产率为46.2%.结论:本实验工艺可以制备高纯度红景天苷,主要降低了生产成本,并对于工业化生产高纯度红景天苷提供一定参考作用.
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| 关 键 词： | 红景天苷 糖苷化 合成 |
The Process Research of Salidroside |
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| XU Li-feng,CAO Di,JIANG Fan,LI Meng,NING Bao-ru,SONG Yang,WANG.The Process Research of Salidroside[J].Journal of Liaoning University(Natural Sciences Edition),2014(1):71-75. |
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| Authors: | XU Li-feng CAO Di JIANG Fan LI Meng NING Bao-ru SONG Yang WANG |
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| Institution: | Qi ( College of Pharmacy, Liaoning University, Shenyang 110036, China) |
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| Abstract: | OBJECTIVE In order to prepare high purity of salidroside, reduce production cost, in this paper, we studied new method for chemosynthesis of salidroside. METHODS To get salidroside, this experiment with the hydroxy benzene ethanol as raw material by glycosidic reaction. RESULTS By high performance liquid chromatography （HPLC） testing, the purity of salidroside is 98.5 %. CONCLUSION The experimental method can prepare high purity rhodiola glucoside and reduce production cost, and provide certain reference for the industrialized production of high purity salidroside. |
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| Keywords: | salidroside glycosylation chemical synthesis method |
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