| 氯乙酸异丙酯的催化合成 |
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| 引用本文： | 牛梅菊,薛建. 氯乙酸异丙酯的催化合成[J]. 聊城大学学报(自然科学版), 2003, 16(3): 37-38,99 |
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| 作者姓名： | 牛梅菊 薛建 |
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| 作者单位： | 1. 聊城大学,化学化工学院,山东,聊城,252059
2. 浙江工业大学,浙江,杭州,310000 |
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| 摘 要： | 以氯乙酸和异丙醇为原料，氯化亚锡为催化剂，合成了氯乙酸异丙酯．探索了酸醇摩尔比、反应时间、催化剂用量等因素对酯化反应的影响，优化出最佳工艺条件并得到较高的酯收率．
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| 关 键 词： | 氯乙酸异丙酯 氯乙酸 异丙醇 催化剂 氯化亚锡 催化合成 酯化反应 氯化亚锡 |
| 文章编号： | 1007-8304(2003)03-0037-02 |
Catalytic Synthesis of Isopropyl Chloroacetate |
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| NIU Mei-ju,XUE Jian. Catalytic Synthesis of Isopropyl Chloroacetate[J]. JOURNAL OF LIAOCHENG UNIVERSITY (NATURAL SCIENCE, 2003, 16(3): 37-38,99 |
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| Authors: | NIU Mei-ju XUE Jian |
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| Abstract: | Isopropyl Chloroacetate was synthesized by esterification of chloroacetatic acid with iso-propyl alcohol in the presence of catalyst stannous chloride. The effects such as acid/alcohol mole ration, catalyst amount and reaction time on esterification conversion were discussed in detail,the optional condition of reaction was obtained and a fairly high ester yield was achieved. |
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| Keywords: | isopropyl chloroacetate stannous chloride catalytic synthesis |
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