| 十六胺乙基磺酸钠的合成和性能研究 |
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| 引用本文： | 葛虹,邵华锋,许培援.十六胺乙基磺酸钠的合成和性能研究[J].北京工商大学学报(自然科学版),2008,26(2):19-22. |
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| 作者姓名： | 葛虹 邵华锋 许培援 |
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| 作者单位： | 郑州轻工业学院,材料与化工学院,河南,郑州,450002 |
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| 摘 要： | 以十六胺和溴乙磺酸钠为原料合成了十六胺乙基磺酸钠,用单因素优选法研究了影响反应的因素,优化反应条件为n(十六胺)∶n(溴乙磺酸钠)=1.0∶1.3,反应温度80℃,反应时间7.0h,pH值9.0~10.0,产物质量收率89.64%,提纯后纯度93.25%,并对十六胺乙基磺酸钠的应用性能进行了测定.
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| 关 键 词： | 十六胺乙基磺酸钠 十六胺 溴乙磺酸钠 |
| 文章编号： | 1671-1513(2008)02-0019-04 |
| 修稿时间： | 2007年12月13 |
SYNTHESIS AND PROPERTY OF SODIUM -2-(N-HEXADECYL) AMINO ETHYL SULFONATE |
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| GE Hong,SHAO Hua-feng,XU Pei-yuan.SYNTHESIS AND PROPERTY OF SODIUM -2-(N-HEXADECYL) AMINO ETHYL SULFONATE[J].Journal of Beijing Technology and Business University:Natural Science Edition,2008,26(2):19-22. |
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| Authors: | GE Hong SHAO Hua-feng XU Pei-yuan |
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| Abstract: | The sodium-2-(N-hexadecyl) amino ethyl sulfonate was synthesized from hexadecyl amine and sodium 2-byomoethyl sulfonate.The factors of its synthesis were studied in detail.The optimum conditions were obtained as follows:the molar ratio of hexadecyl amine: sodium 2-bromoethyl sulfonate=1.0∶1.3,reaction temperature 80 ℃,reaction time 7.0 h,pH 9.0～10.0,the yield of SHES is 89.64% and its purity is 93.25%.The application properties of SHES were measured. |
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| Keywords: | sodium-2-(N-hexadecyl)amino ethyl sulfonate hexadecyl amine sodium 2-bromoethyl sulfonate |
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