| 二糠叉环已酮的制备 |
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| 引用本文： | 李慧章,常成泽,张新华.二糠叉环已酮的制备[J].河北大学学报(自然科学版),1991(2). |
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| 作者姓名： | 李慧章 常成泽 张新华 |
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| 作者单位： | 河北大学化学系
(李慧章，常成泽)，河北大学化学系(张新华) |
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| 摘 要： | 本文介绍了由糠醛和环已酮反应制备二糠叉环已酮的方法以及反应条件的影响。研究了产物薄层色谱的展开体系,选择石油醚:乙醚(1:2)是适宜的。
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| 关 键 词： | 二糠叉环已酮 制备 薄层色谱 |
Preparation of Difurfurylidenecyclohexanone |
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| LiHuizhang Chang Chengze Zhang Xinhua.Preparation of Difurfurylidenecyclohexanone[J].Journal of Hebei University (Natural Science Edition),1991(2). |
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| Authors: | LiHuizhang Chang Chengze Zhang Xinhua |
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| Institution: | Department of chemistry |
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| Abstract: | The title compund was Obtained in 90% yield by condensation of furfuryl with cyclohexanone in a 2:1molar ratio in the presence of 6% aq.NaOH and was analyzed by TLC,IR and NMR. |
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| Keywords: | difurfurylienecyclohexanone preparation TLC |
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