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提取萹蓄总黄酮化学实验及测定
引用本文:曲长明,斯琴毕力格,刘明亮,李增春.提取萹蓄总黄酮化学实验及测定[J].内蒙古民族大学学报(自然科学版),2008,23(3):265-268.
作者姓名:曲长明  斯琴毕力格  刘明亮  李增春
作者单位:[1]内蒙古民族大学化学学院,内蒙古通辽028043 [2]通辽市实验中学,内蒙古通辽028000
基金项目:内蒙古自治区教育厅高校自然科学基金项目(NJ02070)
摘    要:通过对提取蔚蓄总黄酮的微型化学实验法(恒压分液漏斗)与常规实验法(超声波、索氏提取器)比较,实验证明微型化学实验法与常规实验法相比较,该方法具有使用试剂量小、污染小、省时间.适合选做天然有机物的提取化学实验.对所提取的黄酮类物质进行验证,用分光光度法测定含量.微型化学实验法提取蔚蓄总黄酮,测得品中总黄酮的平均含量为1.96%,平均回收率为101%.

关 键 词:蔚蓄  总黄酮  化学实验  分光光度法

Chemistry Experiments about Withdrawing and Determination of Total Flavanone of Polygonum Aviculare L
Institution:QU Chang - ming, Siqinbilig, LIU Ming - liang, LI Zeng - chun ( 1. College of Chemistry, Inner Mongolia University for Nationalities, Tongliao 028043, China; 2. Tongliao City Experimental Middle School, Tongliao 02S000,Chlna )
Abstract:Through extracting Total Flavanone of Polygonum aviculare L the micro scale chemical experiments (constant pressure separating funnel) compared with the traditional method (supersonic wave and apparatus), a new method based on the micro scale chemical experiments compared with the traditional method ,the new method have the characteristics of less pollution, small sample volume and save time. Micri chemical experiments are good ones that are acceptable . Using spectrophotome try to extract and check the flavanone of polygonum aviculare L. Extracting Total Flavanone of Polygonum aviculare L the micro scale chemical experiments, measure sample in average content of the total flavonoid is 1.96%, average recovery rate is 101%.
Keywords:Polygonum aviculare L  Total flavanone  Chemistry Experiments  Spectrophotome
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