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南海七种海藻的多糖组成分析
引用本文:张颖,黄日明,洪爱华,伍秋明,岑颖洲.南海七种海藻的多糖组成分析[J].暨南大学学报,2006,27(3):455-459.
作者姓名:张颖  黄日明  洪爱华  伍秋明  岑颖洲
作者单位:1. 暨南大学化学系,广东,广州,510632
2. 暨南大学实验技术中心,广东,广州,510632
基金项目:广东省科技专项基金;广东省自然科学基金
摘    要:采用3种不同的柱前衍生化方法分别对海藻多糖的水解产物进行前处理,并用GC-MS法分析该海藻多糖的单糖组成.比较可知,糖腈乙酸酯衍生化法的效果最佳.应用该前处理方法对海带、亨氏马尾藻、孔石莼、刺松藻、小石花菜、龙须菜和蜈蚣藻等7种海藻多糖的单糖组成及含量进行了分析可知,以上海藻多糖均含有半乳糖,大多数含有木糖,且海带、亨氏马尾藻和蜈蚣藻多糖含有岩藻糖.

关 键 词:海藻多糖  气质联用  单糖组成
文章编号:1000-9965(2006)03-0455-05
修稿时间:2005年11月4日

Study on monosaccharide composition of seven kinds of algae polysaccharides from the South China Sea
ZHANG Ying,HUANG Ri-ming,HONG Ai-hua,WU Qiu-ming,CEN Ying-zhou.Study on monosaccharide composition of seven kinds of algae polysaccharides from the South China Sea[J].Journal of Jinan University(Natural Science & Medicine Edition),2006,27(3):455-459.
Authors:ZHANG Ying  HUANG Ri-ming  HONG Ai-hua  WU Qiu-ming  CEN Ying-zhou
Abstract:Seven kinds of algae polysaccharides were identified and analyzed by gas chromatograpy-selected mass spectrometry(GC-MS).Derivatization methods were used to study the monosaccharide composition.By comparison,the aldononitrile acetate derivatization is the best method for the analysis of algae polysaccharides.Algae polysaccharides including Laminaria japonica Aresch,Sargassum henslowianum C. Agardh,Ulva pertusa Kjellm,Codium fragile(Sur.) Hario,Gelidium divaricatum Martens,Gracilaria lemaneiformis(Bory) W.v.B,Grateloupia filicina(L.) C.Ag were identified by using this method,it can be concluded that seven algae polysaccharides also have galactose,most of them have xylose,and only Laminaria japonica Aresch,Sargassum henslowianum C.Agardh and Grateloupia filicina(L.) C.Ag have glucose.
Keywords:algal polysaccharide  GC-MS  monosaccharide composition
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