Effects of Coagulation Conditions on Tensile Properties of Regenerated Cellulose Fibers |
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Authors: | YUAN Bin-lan ZHANG Shuai ZHAO Shi-ying LI Fa-xue YU Jian-yong GU Li-xia |
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Affiliation: | 1. Key Laboratory of Textile Science & Technology,Ministry of Education,Shanghai 201620,China;College of Textiles,Donghua University,Shanghai 201620,China 2. Modern Textile Institute,Donghua University,Shanghai 200051,China 3. College of Material Science and Engineering,Donghua University,Shanghai 201620,China |
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Abstract: | The effects of coagulation conditions on tensile properties of the regenerated cellulose fibers prepared by wet-spinning from NaOH/thiourea/urea (8:6.5:8 by weight) aqueous solvent were investigated by tensile tester, X-ray diffraction (XRD), and scanning electron microscope (SEM). The results show that the tensile properties of the as-spun fibers change with the coagualtion concentration, temperature, and time. When the spinning solution is coagulated in 10% H2SO4/12.5% Na2SO4 aqueous solution, the as-spun fibers have a typical structure of cellulose Ⅱ, a circular cross-section, and homogeneous morphological structure. |
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Keywords: | regenerated cellulose fibers NaOH/ thiourea/ urea solvent wet-spinning coagulant |
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