| 3-三氟甲基-4-氨基-5-巯基-1，2，4-三氮唑Schiff碱的微波成合成及表征 |
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| 引用本文： | 李清寒,崔浩,王苗苗.3-三氟甲基-4-氨基-5-巯基-1，2，4-三氮唑Schiff碱的微波成合成及表征[J].西南民族学院学报(自然科学版),2009,35(5):1037-1040. |
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| 作者姓名： | 李清寒 崔浩 王苗苗 |
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| 作者单位： | 西南民族大学化学与环境保护工程学院,四川成都,610041 |
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| 基金项目： | 西南民族大学青年重点项目，西南民族大学学生创新项目 |
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| 摘 要： | 以3-三氟甲基-4-氨基-1，2，4-三氮唑-5-硫酮和取代苯甲醛为起始原料，在微波辐射下，经缩合反应制得了7个Schi行碱3（a—g）．合成的7个目标化合物通过熔点测定和质谱、红外光谱、核磁共振氢谱分析、元素分析对其结构进行确证．
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| 关 键 词： | Schiff碱 三唑硫酮 有机合成 微波辐射 |
Microwave-assisted synthesis and characterization of trifluoromethyl substituted triazolethione Schiff base |
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| LI Qing-han,CUI Hao,WANG Miao-miao.Microwave-assisted synthesis and characterization of trifluoromethyl substituted triazolethione Schiff base[J].Journal of Southwest Nationalities College(Natural Science Edition),2009,35(5):1037-1040. |
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| Authors: | LI Qing-han CUI Hao WANG Miao-miao |
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| Institution: | (School of Chemistry and Environmental Protection Engineering, Southwest University for Nationalities, Chengdu 610041, P.R.C.) |
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| Abstract: | Under microwave irradiation conditions, seven Scbiff bases 3（a-g） have been synthesized using 3-trifluoromethyl-4-amino-1, 2,4-triazole-5-thione and substituted benzaldehyde as starting mateials. The structures of seven compounds have been confirmed by IR, ^1H NMR, MS spectra and elemental analysis. All these results have offered some important reference to systematic study on 1,2,4-triazole Schiffbase compounds in the future. |
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| Keywords: | Schiff base triazolethione organic synthesis microwave irradiation |
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