| 1，3-丙二醇的合成及其结构表征 |
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| 引用本文： | 彭本军,曾艳.1，3-丙二醇的合成及其结构表征[J].淮北煤师院学报,2009(1):50-54. |
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| 作者姓名： | 彭本军 曾艳 |
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| 作者单位： | 淮北煤炭师范学院化学与材料科学学院,安徽淮北235000 |
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| 摘 要： | 文章以无水乙酸钠、3-溴-1-氯丙烷、苄基三乙基氯化铵、无水甲醇、717#离子交换树脂等为原料合成1，3-丙二醇，并对合成的产物用红外光谱、氢核磁共振波谱进行分析检测．
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| 关 键 词： | 1 3-丙二醇 3-溴-1-氯丙烷 苄基三乙基氯化铵 相转移催化剂 |
The Synthesis and Structural Measurement of 1, 3 -propanediol |
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| PENG Ben-jun,ZENG Yan.The Synthesis and Structural Measurement of 1, 3 -propanediol[J].Journal of Huaibei Teachers College(Natural Sciences Edition),2009(1):50-54. |
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| Authors: | PENG Ben-jun ZENG Yan |
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| Institution: | ( School of Chemistry and Material Science, Huaibei Coal Industry Teachers College, 235000, Huaibei, Anhui, China) |
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| Abstract: | In this paper, 1, 3-propanediol is synthesized using anhydrous sodium acetate, 3-bromo-l-chloropropane, anhydrous methanol, benzyl triethyl ammonium chloride and anion exchange resin etc. as materials. In addition, infrared spectra and hydrogen nuclear magnetic resonance are used to determine the chemical structure of production. |
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| Keywords: | 1 3-propanediol 3-bromo-1-chloropropane benzyl triethyl ammonium chloride phase transfer catalyst |
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