| 凤丹牡丹花瓣化学成分研究 |
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| 引用本文： | 凤丹牡丹花瓣化学成分研究.凤丹牡丹花瓣化学成分研究[J].山东科学,2017,30(3):12-16. |
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| 作者姓名： | 凤丹牡丹花瓣化学成分研究 |
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| 作者单位： | 1.山东省中药质量控制重点实验室，山东省分析测试中心，山东 济南 250014； 2.烟台出入境检验检疫局，山东 烟台 264000 3.山东中医药大学药学院，山东 济南 250014 |
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| 基金项目： | Paeonia suffruticosa Andr. cv. Fengdan|flower petals|gallotannins|flavonoid |
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| 摘 要： | 对凤丹牡丹花瓣化学成分进行深入研究,运用高效液相色谱方法进行分离纯化,运用1H NMR、13C NMR和MS波谱学数据鉴定其结构。结果得到2个没食子酸鞣质类化合物,分别为1-O-galloyl-β-D-glucose(1)和1,2,3,4,6-Trigalloyl-β-D-glucose(2),以及一个黄酮类化合物kaempferol-3,7-di-O-β-D-glucopyranoside(3)。化合物1~3均首次从凤丹牡丹花中分离得到,化合物1~2也是首次从凤丹牡丹花中分离得到鞣质类化合物。
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| 关 键 词： | 牡丹 鞣质 黄酮 花瓣 |
Research on tannins and flavonoid from the flowerpetals of Paeonia suffruticosa Andr. cv. Fengdan |
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| YAN Hui-jiao,WANG Zhi-wei,CHEN Yan-ping,JIANG Jiao-Jiao,CUI Li,GENG Yan-ling,WANG Xiao.Research on tannins and flavonoid from the flowerpetals of Paeonia suffruticosa Andr. cv. Fengdan[J].Shandong Science,2017,30(3):12-16. |
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| Authors: | YAN Hui-jiao WANG Zhi-wei CHEN Yan-ping JIANG Jiao-Jiao CUI Li GENG Yan-ling WANG Xiao |
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| Institution: | 1.Shandong Analysis and Test Center,Shandong Key Laboratory Breeding Base of TCM Quality Control Technology,Jinan 250014,China; 2.Yantai Entry Exit Inspection and Quarantine Bureau,Yantai 264000,China； 3.School of Pharmaceutical Sciences, Shandong University of Traditional Chinese Medicine,Jinan 250014,China |
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| Abstract: | In this paper, the chemical constituents from the flower petals of Paeonia suffruticosa Andr. cv. Fengdan were thoroughly studied, which were isolated and purified by HPLC, and identified by 1H NMR、13C NMR and MS. Two gallotannins both 1-O-galloyl- β-D-glucose (1) and 1, 2, 3, 4, 6 Trigalloyl- β-D-glucose (2), as well as a flavonoid kaempferol-3,7-di-O- β-D-glucopyranoside (3) were isolated from the flower petals of Paeonia suffruticosa Andr. cv. Fengdan by HPLC methods. Compounds 1~3 were all obtained from the flowers of Paeonia suffruticosa Andr. cv. Fengdan for the first time, and Compounds 1~2 were also the tannins obtained from this genus for the first time. |
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