| 沙棘果硫酸化酯多糖HR_3SL的制备与分析 |
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| 引用本文： | 张丽萍,陈玉香,刘立东,陈少刚. 沙棘果硫酸化酯多糖HR_3SL的制备与分析[J]. 东北师大学报(自然科学版), 1999, 0(3) |
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| 作者姓名： | 张丽萍 陈玉香 刘立东 陈少刚 |
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| 作者单位： | 东北师范大学生命科学学院!吉林长春130024(张丽萍，刘立东，陈少刚)，吉林工业大学食品与包装工程学院!吉林长春130024(陈玉香) |
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| 摘 要： | 从沙棘果皮分离提取了相对分子质量较均一的杂多糖ＨＲ３ ．用氯碘酸吡啶法对ＨＲ３ 进行硫酸化修饰后，相对分子质量明显增大，ＨＲ３ＳＬ的紫外光谱与红外光谱分析表明，在２０８ ｎｍ ，２６８ ｎｍ ，２８６ ｎｍ 和１ ２４０ ｃｍ －１ ，６２０ ｃｍ －１ 有硫酸酯键的特征吸收峰．紫外光谱法与硫酸钡质量法测定ＨＲ３ＳＬ中ＳＯ２－４ 含量约为２１ ％ ．
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| 关 键 词： | 沙棘多糖 沙棘 硫酸化 |
Synthesis and analysis of polysacchrivide sulfate from the fruits of Hippophae rhamnoides L. |
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| ZHANG Li ping ,CHEN Yu xiang ,LIU Li dong ,CHEN Shao gang. Synthesis and analysis of polysacchrivide sulfate from the fruits of Hippophae rhamnoides L.[J]. Journal of Northeast Normal University (Natural Science Edition), 1999, 0(3) |
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| Authors: | ZHANG Li ping CHEN Yu xiang LIU Li dong CHEN Shao gang |
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| Affiliation: | ZHANG Li ping 1,CHEN Yu xiang 2,LIU Li dong 1,CHEN Shao gang 1 |
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| Abstract: | Polysaccharide HR 3 was isolated from the fruits of Hippophae rhamnoides L. HR 3SL was obtained from sulfational modification of HR 3 ith chlorosulfonic acid-pyridine. The UV and IV spectrum of HR 3SL showed absorptions of sulfati ester bonde at 218?nm,264?nm,268?nm,286?nm and 1?240?cm -1 ,620?cm -1 respectively. Analysis of UV and BaSO 4 weight showed HR 3SL contained SO -2 4 about 21%. |
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| Keywords: | polysaccharide Hippohae rhamnoides L. sulfation |
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