| 高效液相色谱法测定蔬菜中噻苯咪唑残留量 |
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| 引用本文： | 吴发远,徐亚英,苗兴芬. 高效液相色谱法测定蔬菜中噻苯咪唑残留量[J]. 中国西部科技, 2011, 10(8): 12-12,7. DOI: 10.3969/j.issn.1671-6396.2011.08.005 |
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| 作者姓名： | 吴发远 徐亚英 苗兴芬 |
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| 作者单位： | 黑龙江农业职业技术学院,黑龙江,佳木斯,154007 |
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| 摘 要： | 研究目的:采用高效液相色谱法对蔬菜中噻苯咪唑进行分离和检测。方法:蔬菜样品经甲醇提取,高速离心沉淀分离后,以甲醇+水(50+50)为流动相,采用C柱(3.9mm×150mm×5μm)分离,流速为1.0mL/min,UV300nm检测。结果:该方法所测得的噻苯咪唑在0～20.0mg/L内具有良好的线性特征,检出限为0.01mg/kg。结论:该方法适合各种蔬菜农药残留量的分析。
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| 关 键 词： | 高效液相色谱 蔬菜 噻苯咪唑 |
Determination of Residual Amount of Thiabendazole in Vegetable by High Performance Liquid Chromatography |
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| WU Fa-yuan,XU Ya-ying,IAO Xing-fen. Determination of Residual Amount of Thiabendazole in Vegetable by High Performance Liquid Chromatography[J]. Science and Technology of West China, 2011, 10(8): 12-12,7. DOI: 10.3969/j.issn.1671-6396.2011.08.005 |
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| Authors: | WU Fa-yuan XU Ya-ying IAO Xing-fen |
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| Affiliation: | WU Fa-yuan,XU Ya-ying,MIAO Xing-fen(College of Hei Longjiang Agricultural Vocation and Technology,Hei longjiang,Jiamusi 154007) |
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| Abstract: | OBJECTIVE,Residues of thiabendazole in vegetables were analyzed and separated by high performance liquid chromatography.METHOD,C18 column（3.9mm×150mm×5μm）,the mobile phase：CH3OH＋H2O（50＋50）,the flow rate：1.0 ml/min,the UV detector wave length：300nm.RESULTS,The experimental data had a good characteristic of linearity in the range of 0～20.0mg/L with the detecting limit0.01mg/kg.CONCLUSION,The method could be used to analyze pesticide in different vegetables. |
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| Keywords: | High performance liquid chromatography Vegetable Thiabendazole |
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