| Pb_2SnO_4的新型合成方法 |
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| 引用本文： | 李秀玲,吴明姆,罗裕基.Pb_2SnO_4的新型合成方法[J].徐州师范大学学报(自然科学版),1999(1). |
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| 作者姓名： | 李秀玲 吴明姆 罗裕基 |
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| 作者单位： | 徐州师范大学化学系，中山大学化学系 |
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| 摘 要： | 首次分别在ＳｎＣｌ４－Ｐｂ（ＮＯ３）２－ＮａＯＨ－Ｈ２Ｏ和ＰｂＡｃ２－Ｎａ２ＳｎＯ３－ＮａＯＨ－Ｈ２Ｏ两个水热体系中一步合成了四方锡酸铅（Ｐｂ２ＳｎＯ４）晶体，条件温和，方法简单，易控，节能，ＸＲＤ和ＳＥＭ结果表明产物为单晶，相纯度高且形貌完美．
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| 关 键 词： | 水热法 锡酸铅 结晶度 |
A New Synthesis Method of Tetragonal Lead Stannate (Pb 2SnO 4) |
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| LI Xiu ling ,WU Ming mei ,LUO Yu ji.A New Synthesis Method of Tetragonal Lead Stannate (Pb 2SnO 4)[J].Journal of Xuzhou Normal University(Natural Science Edition),1999(1). |
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| Authors: | LI Xiu ling WU Ming mei LUO Yu ji |
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| Institution: | LI Xiu ling 1,WU Ming mei 2,LUO Yu ji 2 |
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| Abstract: | Tetragonal lead stannate (PbSnO 4) was synthesized in two hydrothermal systems of SnCl 4 Pb(NO 3) 2 NaOH H 2O and PbAc 2 Na 2SnO 3 NaOH H 2O respectively by one step with mild,simple,controllable condition and lower energy consumption.The result of XRD and SEM shows that it is single crystal with pure phase and perfect morphology. |
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| Keywords: | hydrothermal method lead stannate crystallinity |
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