| 超声辐射下合成N’-三氮唑-N-取代 苯氧乙酰基硫脲 |
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| 引用本文： | 李淑贤,李雅,许文峰,申利红.超声辐射下合成N’-三氮唑-N-取代 苯氧乙酰基硫脲[J].河北大学学报(自然科学版),2011,31(4):397-400. |
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| 作者姓名： | 李淑贤 李雅 许文峰 申利红 |
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| 作者单位： | 邯郸学院化学系,河北邯郸,056005 |
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| 基金项目： | 河北省科技计划项目，邯郸市科学技术研究与发展计划项目 |
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| 摘 要： | 为给药物筛选提供先导化合物,利用超声波与相转移催化联用技术,合成了3个N’-三氮唑-N-取代苯氧乙酰基硫脲衍生物,其结构经元素分析,IR和1 H NMR进行了表征.该法具有操作简单、反应时间短等优点.初步的生物活性测试表明:部分化合物具有一定的除草活性.
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| 关 键 词： | 酰基硫脲 三氮唑 超声辐射 |
Synthesis of N'-triazolyl-N-substituted Phenoxyacetyl Thioureas Under Ultrasound |
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| LI Shu-xian,LI Ya,XU Wen-feng,SHEN Li-hong.Synthesis of N'-triazolyl-N-substituted Phenoxyacetyl Thioureas Under Ultrasound[J].Journal of Hebei University (Natural Science Edition),2011,31(4):397-400. |
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| Authors: | LI Shu-xian LI Ya XU Wen-feng SHEN Li-hong |
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| Institution: | (Department of Chemistry,Handan College,Handan 056005,China) |
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| Abstract: | Three new N-triazolyl-N'-substituted phenoxyacety thioureas were designed and synthesized by combined technique of ultrasonic irradiation and phase transfer catalysis.The structures of target compounds were characterized by elemental analysis,IR and 1H NMR.The synthetic method has the advantages of simple operation and short time.The preliminary biological test shows that some of compounds have some inhibitory against weeds. |
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| Keywords: | thioureas triazol ultrasonic irradiation |
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