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微波制备沸石负载N/TiO_2光降解催化剂及对罗丹明B的降解
作者单位:;1.信阳师范学院化学化工学院
摘    要:以沸石为载体,以钛酸丁酯和尿素为助剂,采用溶胶-凝胶法制备沸石负载N/TiO2光降解催化剂.在可见光下对罗丹明B进行降解实验,讨论影响罗丹明B降解性能的主要因素.结果表明,当微波反应15min,焙烧温度为450℃、催化剂用量为40 mg/L、光照时间为30 min时,样品对罗丹明B的降解率可达99.2%以上.光降解催化剂再生后重复使用4次,降解率仍可达89.7%.

关 键 词:微波  沸石  负载  氮/TiO2  罗丹明B

Microwave Preparation Zeolite Loading N/TiO_2 Photocatalysts and Its Photodegradation on Rhodaminc B
Institution:,College of Chemistry and Chemical Engineering,Xinyang Normal University
Abstract:The nitrogen-doped TiO2 photocatalysts were prepared by sol-gel method,using trtrabutyl titanate and carbamide as raw materials and zeolite as the supporter.The major factors were tested and discussed to photocatalyst degradation of rhodamine B in the sunlight.The results showed that after the microwave reaction was conducted for 15 min,the rhodamine B degradation rate of 30 min may reach above 99.2%in visible light when the dosage of 40mg/L and the roasting temperature was 450℃.The degradation rate could reach 89.7%after the photocatalyst was regenerated for 4times
Keywords:microwave  zeolite  load  N/TiO2  rhodaminc B
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