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溶胶-凝胶法制备镍酸镧薄膜的研究
引用本文:魏凌,张丽亭.溶胶-凝胶法制备镍酸镧薄膜的研究[J].淮阴师范学院学报(自然科学版),2006,5(2):117-120.
作者姓名:魏凌  张丽亭
作者单位:河南大学,物理与信息光电子学院,河南,开封,475001
摘    要:采用溶胶-凝胶(sol-gel)法,使用浓度分别为0.1 mol/L、0.2 mol/L和0.3 mol/L的前驱体溶液,在单晶Si(100)衬底上制备了镍酸镧LaNiO3](简称LNO)导电薄膜,研究了前驱体溶液浓度对LNO薄膜结构和导电性能的影响.X射线衍射测试表明,三种样品均为纯的钙钛矿相,具有较好的(110)择优取向.原子力显微镜分析显示,用0.2 mol/L前驱体溶液制备的LNO薄膜样品晶粒明显大于0.1 mol/L的样品.采用标准四探针法测试了三种样品的电阻率,当前驱体溶液浓度为0.2 mol/L时,样品电阻率最小,仅为2.08×10-3Ω.cm,具有良好的导电性.

关 键 词:溶胶-凝胶法  前驱体溶液  LaNiO3  电阻率
文章编号:1671-6876(2006)02-0117-04
收稿时间:2006-01-06
修稿时间:2006年1月6日

Study on the Preparation of LaNiO3 Thin Films Using Sol-gel Method
WEI Ling,ZHANG Li-ting.Study on the Preparation of LaNiO3 Thin Films Using Sol-gel Method[J].Journal of Huaiyin Teachers College(Natrual Science Edition),2006,5(2):117-120.
Authors:WEI Ling  ZHANG Li-ting
Abstract:LaNiO_3(LNO) thin films were prepared on Si(100) substrates by a sol-gel method.We investigated the effect of precursor concentration on the structure and the conductivity of LNO films.The XRD results showed that all of the samples were of pure perovskite structure and of high(110)-orientation.AFM analysis showed that the crystallite size of the 0.2M-LNO film was biger than 0.1M-LNO film obviously.Among these three samples,the 0.2 M-LNO film displayed the lowest resistivity of 2.08×10~(-3)Ω·cm.
Keywords:sol-gel  precursor  concentration  LaNiO_3  resistivity
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