| 对羟基苯甲酸法合成对羟基苯甲腈及产物分析 |
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| 引用本文： | 郭一锋,陈平.对羟基苯甲酸法合成对羟基苯甲腈及产物分析[J].广西科学院学报,2010,26(3):228-229. |
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| 作者姓名： | 郭一锋 陈平 |
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| 作者单位： | 1. 桂林理工大学材料学院,广西桂林,541004
2. 桂林理工大学材料学院,广西桂林,541004;有色金属及材料加工教育部重点实验室,广西桂林,541004 |
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| 摘 要： | 以对羟基苯甲酸和尿素为基本原料,在脱水剂和催化剂共同作用下,直接酰胺化一锅法合成对羟基苯甲腈,并采用熔点测定和红外分析方法判定产物结构。
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| 关 键 词： | 对羟基苯甲腈 酰胺反应 一锅法 |
| 收稿时间： | 2010/6/28 0:00:00 |
Synthesis and IR Analysis of 4-Hydroxybenzonitrile |
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| GUO Yi-feng and CHEN Ping.Synthesis and IR Analysis of 4-Hydroxybenzonitrile[J].Journal of Guangxi Academy of Sciences,2010,26(3):228-229. |
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| Authors: | GUO Yi-feng and CHEN Ping |
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| Institution: | 1.Faculty of Material Science ＆ Engineering,Guilin University of Technology,Guilin,Guangxi,541004,China;2.Key Laboratory of New Processing Technology for Nonferrous Metals and Materials Constituted by Ministry of Education,Guilin University of Technology,Guilin,Guangxi,541004,China) |
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| Abstract: | 4-Hydroxybenzonitrile,which is one important fine chemical intermediates,was synthesized by 4-hydroxybenzonic acid and urea through acylating reaction and dehydrating reaction.The structure of 4-hydroxybenzonitrile was characterized by FT-IR and melt-point analysis. |
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| Keywords: | 4-Hydroxybenzonitrile acylating reaction one-Pot Synthesis |
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