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| 微量进样-火焰原子吸收分光光度法测定红细胞以及其它组织中的铅 | |
| 引用本文： | 马登军,孙汉文,柳松,吴发超,袁倬斌.微量进样-火焰原子吸收分光光度法测定红细胞以及其它组织中的铅[J].华北科技学院学报,2008,5(4):52-55. |
| 作者姓名： | 马登军 孙汉文 柳松 吴发超 袁倬斌 |
| 作者单位： | 1. 华北科技学院,环境工程系,北京东燕郊,101601;河北大学,化学与环境学院,河北保定,071002;中国科学院研究生院,化学与化学工程学院,北京,100083 2. 河北大学,化学与环境学院,河北保定,071002 3. 华北科技学院,环境工程系,北京东燕郊,101601 4. 中国科学院研究生院,化学与化学工程学院,北京,100083 |
| 基金项目： | 国家自然科学基金分析化学重点基金，国际合作基金，中科院长春应化所电分析化学国家重点实验室基金，中科院研究生院院长基金，华北科技学院基金 |
| 摘 要： | 在国产GGX-600型原子吸收分光光度计上采用微量进样技术，用火焰原子吸收光谱法测定了小白鼠红细胞、血清、肝、肾、脾、肺、心脏和大脑中铅的含量。实验结果表明该方法铅在0．050～1．000μg／mL呈良好线性关系，r=0．9997，方法平均回收率97．4％，RSD=4．2％，特征浓度为0．0916μg/mL，检出限为0．0500μg／mL。方法操作简单，重现性好，结果准确且待测样品用量少。 |
| 关 键 词： | 铅 微量进样 火焰原子吸收光谱 血红细胞 |
Determination of Lead in Blood Red Cell and Other Target Organ by Flame Atomic Absorption Spectrophotometry with Micro-Sampling |
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| MA Deng-jun,SUN Han-wen,LIU Song,WU Fa-chao,YUAN Zhuo-bin.Determination of Lead in Blood Red Cell and Other Target Organ by Flame Atomic Absorption Spectrophotometry with Micro-Sampling[J].Journal of North China Institute of Science and Technology,2008,5(4):52-55. | |
| Authors: | MA Deng-jun SUN Han-wen LIU Song WU Fa-chao YUAN Zhuo-bin |
| Institution: | MA Dengjun~(1,2,3) SUN Hanquan~2 LIU Song~1 WU Fachao~1 YUAN Zhuobin~3 (1.North China Institute of Science , Technology,Yaojiac Beijing-east 101601,2.Institute of Chemistry , Environment Hebei University,Baoding Hebei 071002,3.College of Chemistry , Chemical Engineering,the Graduate University of th Chinese Academy of Sciences,Beijing 100083) |
| Abstract: | In this paper, the determination of Pb in Blood Red Cell, Blood Plasma, Liver, Kidney, Spleen, Lung, Heart and Cerebrum by Flame Atomic Absorption Spectrophotometry with micro-Sampling is described. An average recovery of 97.4% was obtained with a RSD of 4. 2% and r = 0. 9997 in the range of 0. 050-1. 000μg/mL. The detection lime it was 0. 0500 μg/mL. The proposed method offers simple instrumental operation, good reproducibility, accuracy and Sample use less |
| Keywords: | Lead micro-sampling flame atomic absorption spectrophotometry blood red cell |
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