| 呋喃丙烯酸酯类香料的合成与研究 |
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| 引用本文： | 张维成,孙宝国,徐理阮. 呋喃丙烯酸酯类香料的合成与研究[J]. 北京工商大学学报(自然科学版), 1994, 0(1) |
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| 作者姓名： | 张维成 孙宝国 徐理阮 |
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| 作者单位： | 北京轻工业学院化学工程系 |
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| 摘 要： | 本文用正交实验确定了呋喃丙烯酸丙酯合成的最佳条件，并以此为根据，适当改变催化剂浓硫酸的用量，合成了呋喃丙烯酸的甲酯、乙酯、异丙酯、丁酯、异丁酯、戊酯、异戊酯、己酯、庚酯、丙烯酯、环己酯和苯甲酯。通过ＩＲ，￣１Ｈ－ＮＭＲ等分析方法证实了它们的结构，还测定了它们的物理常数沸点、折射率等，并做了评香鉴定。
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| 关 键 词： | 呋喃，呋喃丙烯酸，酯化反应，香料 |
THHE STUDY OF THE SYNTHESIS OF FURANACRYLATE |
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| Zhang Weicheng,Sun Baoguo, Xu Liruan. THHE STUDY OF THE SYNTHESIS OF FURANACRYLATE[J]. Journal of Beijing Technology and Business University:Natural Science Edition, 1994, 0(1) |
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| Authors: | Zhang Weicheng Sun Baoguo Xu Liruan |
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| Abstract: | The better condition of synthesis of propyl ester furanacrylic acid was found by its orthogonal experiment with changing the amount of catalyst of sulfuric acid. The synthesis of methyl, ethyl, propyl, butyl,amyl, hexyl, isopropyl, isobutyl, isoamyl, allyl,cyclohexyl and benzyl ester of furanacrylic acid were completed. The structrues were confirmed by IR, ￣1H-NMR. The physical constants including boiling point, refractive index et. alwere measured too. Aroma appraisal was given by Beijing Liyuan Essence Plant. |
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| Keywords: | Furan Furanacrylic acid Esterification Flavoring |
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