| 4-碘-1H-咪唑的合成工艺研究 |
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| 引用本文： | 沈健芬. 4-碘-1H-咪唑的合成工艺研究[J]. 科学技术与工程, 2011, 11(15): 3498-3500 |
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| 作者姓名： | 沈健芬 |
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| 作者单位： | 台州学院医药化工学院,台州,317000 |
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| 基金项目： | 台州市科技计划项目（No. 0902KY03） |
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| 摘 要： | 以咪唑、碘为原料,经双取代和脱碘反应得到4-碘-1H-咪唑,总收率为73.5%。该方法操作便捷,原料易得,收率高,成本低,各主要化合物结构经核磁共振氢谱确认。
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| 关 键 词： | 4-碘-1H-咪唑 工艺改进 咪唑 |
| 收稿时间： | 2011-02-28 |
| 修稿时间： | 2011-02-28 |
Research on the Synthesis of 4-iodo-1H-imidazole |
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| shen jian fen. Research on the Synthesis of 4-iodo-1H-imidazole[J]. Science Technology and Engineering, 2011, 11(15): 3498-3500 |
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| Authors: | shen jian fen |
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| Affiliation: | L(U) Jin-fen,SHEN Jian-fen,WANG Bin,LEI Hong-xia,ZHENG Ru |
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| Abstract: | 4-iodo-1H-imidazole was prepared from Iodine and imidazole via substitute reaction and deiodination reaction. The staring materials in the synthetic route were easily available and the yield was reasonable. The overall yield was 73.5%. The structures of the main intermediates were identified by 1H NMR. |
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| Keywords: | 4-iodo-1H-imidazole process improvement imidazole |
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