| 环状磷酰基硫脲的合成研究 |
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| 引用本文： | 匡宇明,李中华.环状磷酰基硫脲的合成研究[J].华中师范大学学报(自然科学版),2004,38(1):63-65. |
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| 作者姓名： | 匡宇明 李中华 |
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| 作者单位： | 华中师范大学,化学学院,武汉,430079 |
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| 摘 要： | 采用2-异硫氰基-5，5-二甲基-2-氧代-1，3，2-二氧磷杂环己烷与不同的胺反应合成了13个新型的环状磷酰基硫脲衍生物，它们的结构经^1H NMR、IR和元素分析证实．
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| 关 键 词： | 1，3，2-二氧磷杂环 磷酰基硫脲 合成 |
| 文章编号： | 1000-1190(2004)01-0063-03 |
Studies on the synthesis of cyclophosphorylthioureas |
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| KUANG Yu-ming,LI Zhong-hua.Studies on the synthesis of cyclophosphorylthioureas[J].Journal of Central China Normal University(Natural Sciences),2004,38(1):63-65. |
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| Authors: | KUANG Yu-ming LI Zhong-hua |
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| Abstract: | Thirteen new cyclophosphorylthiourea derivatives,R~1R~2NC(S)NHR~3((R~1=H;)R~2=substituted phenyl;R~3=5,5-dimethyl-2-oxa-1,3,2-dioxaphosphoranyl) were synthesized by the reaction of 2-isothiocyano-5,5-dimethyl-2-oxa-1,3,2-dioxaphosphorinane with various amines respectively, their structures were confirmed by means of ()~1H NMR, IR and elemental analysis. |
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| Keywords: | 1 3 2-dioxaphosphorinane phosphorylthiourea synthesis |
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