| O—取代苯基—O—四氯乙基硫逐磷酰胺酯的合成及生物活性研究 |
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| 引用本文： | 李盛彪,黄天宝.O—取代苯基—O—四氯乙基硫逐磷酰胺酯的合成及生物活性研究[J].湖北大学学报(自然科学版),1996,18(2):150-154. |
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| 作者姓名： | 李盛彪 黄天宝 |
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| 作者单位： | [1]湖北大学化学系 [2]华中师范大学有机合成研究所 |
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| 摘 要： | ＰＣｌ５与Ｃｌ３ＣＣＨＯ加成后在低温下通入干燥的Ｈ２Ｓ／ｇ，可制得Ｃｌ３ＣＣＨＣｌＯＰ（Ｓ）Ｃｌ２（１），（１）依次与取代苯酚、胺反应合成了１２个具有生物活性的标题化合物。用ＩＲ、ＮＭＲ、ＭＳ和元素分析对其结构进行了表征。并讨论了合成方法、波谱性质和生物活性的规律。结果表明该类硫逐磷酰胺的抑制植物生长活性较高，而硫逐磷酸酯的杀虫活性较高。
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| 关 键 词： | 硫逐磷酰胺酯 合成 生物活性 四氯乙基 杀虫剂 |
STUDIES ON THE SYNTHESIS AND BIOLOGICAL ACTIVITY OF O SUBSTITUTED PHENYL O TETRACHLOROETHYL PHOSPHORAMIDOTHIOATES |
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| Li Shengbiao,Huang Shiqiang.STUDIES ON THE SYNTHESIS AND BIOLOGICAL ACTIVITY OF O SUBSTITUTED PHENYL O TETRACHLOROETHYL PHOSPHORAMIDOTHIOATES[J].Journal of Hubei University(Natural Science Edition),1996,18(2):150-154. |
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| Authors: | Li Shengbiao Huang Shiqiang |
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| Abstract: | Twelve new O substituted phenyl O tetrachloroethyl phosphoramidothioates were synthesized. The title compounds have been characterized by IR, MS, NMR and elementary analysis. Their biological activities were tested. The results showed these phosphoramidothioates are better herbicides, and these phosphorothioates are better insecticides. |
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| Keywords: | Phosphoramidotioate Synthesis Biological activity |
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